1-<5-(1,1-dimethylethyl)-3-iodo-2-methoxyphenyl>methylamine hydrochloride

Base Information

Chemical Name:1-<5-(1,1-dimethylethyl)-3-iodo-2-methoxyphenyl>methylamine hydrochloride
CAS No.:81440-85-9
Molecular Formula:C₁₂H₁₈INO*ClH
Molecular Weight:355.646
Hs Code.:

Synonyms:1-<5-(1,1-dimethylethyl)-3-iodo-2-methoxyphenyl>methylamine hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-<5-(1,1-dimethylethyl)-3-iodo-2-methoxyphenyl>methylamine hydrochloride

Chemical Property:

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Technology Process of 1-<5-(1,1-dimethylethyl)-3-iodo-2-methoxyphenyl>methylamine hydrochloride

There total 3 articles about 1-<5-(1,1-dimethylethyl)-3-iodo-2-methoxyphenyl>methylamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: N-(5-tert-Butyl-3-iodo-2-methoxy-benzyl)-2,2,2-trifluoro-acetamide

: 81440-85-9
1-<5-(1,1-dimethylethyl)-3-iodo-2-methoxyphenyl>methylamine hydrochloride

Guidance literature:: With hydrogenchloride; In ethanol; for 2h; Heating;
DOI:10.1021/jm00348a024

Reference yield:

: 58456-91-0
2-aminomethyl-4-tert-butyl-6-iodophenol

: 81440-85-9
1-<5-(1,1-dimethylethyl)-3-iodo-2-methoxyphenyl>methylamine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / 0.25 h / 20 °C

2: K₂CO₃ / dimethylformamide / 4 h / 50 °C

3: 72 percent / conc. HCl / ethanol / 2 h / Heating

With hydrogenchloride; potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00348a024

Reference yield:

: 68967-68-0
2,2,2-trifluoro-N-<<5-(1,1-dimethylethyl)-2-hydroxy-3-iodophenyl>methyl>acetamide

: 81440-85-9
1-<5-(1,1-dimethylethyl)-3-iodo-2-methoxyphenyl>methylamine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide / 4 h / 50 °C

2: 72 percent / conc. HCl / ethanol / 2 h / Heating

With hydrogenchloride; potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00348a024