<(4-chlorophenyl)phenylmethyl>triphenylphosphonium chloride

Base Information

• Chemical Name: <(4-chlorophenyl)phenylmethyl>triphenylphosphonium chloride
• CAS No.: 25361-60-8
• Molecular Formula: C₃₁H₂₅ClP*Cl
• Molecular Weight: 499.419
• Mol file: 25361-60-8.mol

Synonyms:<(4-chlorophenyl)phenylmethyl>triphenylphosphonium chloride

Chemical Property of <(4-chlorophenyl)phenylmethyl>triphenylphosphonium chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of <(4-chlorophenyl)phenylmethyl>triphenylphosphonium chloride

There total 1 articles about <(4-chlorophenyl)phenylmethyl>triphenylphosphonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1-chloro-4-(chloro(phenyl)methyl)benzene (134-83-8,60035-71-4) + triphenylphosphine (603-35-0) → <(4-chlorophenyl)phenylmethyl>triphenylphosphonium chloride (25361-60-8)

Guidance literature:

at 160 ℃; for 6h;

Reference yield:

<(4-chlorophenyl)phenylmethyl>triphenylphosphonium chloride (25361-60-8) → Triphenylphosphine selenide (3878-44-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 67 percent / NaNH₂ / toluene; tetrahydrofuran / Ambient temperature

2: Se / toluene / 8 h / 80 °C

With selenium; sodium amide; In tetrahydrofuran; toluene;

Reference yield:

<(4-chlorophenyl)phenylmethyl>triphenylphosphonium chloride (25361-60-8) → 1,2-bis(4-chlorophenyl)-1,2-diphenylethene

Guidance literature:

Multi-step reaction with 3 steps

1: 67 percent / NaNH₂ / toluene; tetrahydrofuran / Ambient temperature

2: Se / toluene / 8 h / 80 °C

3: toluene / 1) -78 to r.t., during 1h; 2) 50 deg C

With selenium; sodium amide; In tetrahydrofuran; toluene;

upstream raw materials:

1-chloro-4-(chloro(phenyl)methyl)benzene

triphenylphosphine

Downstream raw materials:

Triphenylphosphine selenide

(4-Chloro-phenyl)-phenyl-methaneselone