1-(4-chloro-2,5-dimethoxyphenyl)-3-(3-(propylamino)propyl)thiourea hydrochloride

Base Information

Chemical Name:1-(4-chloro-2,5-dimethoxyphenyl)-3-(3-(propylamino)propyl)thiourea hydrochloride
CAS No.:1276682-54-2
Molecular Formula:C₁₅H₂₄ClN₃O₂S*ClH
Molecular Weight:382.354
Hs Code.:

Synonyms:1-(4-chloro-2,5-dimethoxyphenyl)-3-(3-(propylamino)propyl)thiourea hydrochloride

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Chemical Property of 1-(4-chloro-2,5-dimethoxyphenyl)-3-(3-(propylamino)propyl)thiourea hydrochloride

Chemical Property:

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Technology Process of 1-(4-chloro-2,5-dimethoxyphenyl)-3-(3-(propylamino)propyl)thiourea hydrochloride

There total 4 articles about 1-(4-chloro-2,5-dimethoxyphenyl)-3-(3-(propylamino)propyl)thiourea hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1159074-29-9
tert-butyl 3-(3-(4-chloro-2,5-dimethoxyphenyl)thioureido)propylpropylcarbamate

: 1276682-54-2
1-(4-chloro-2,5-dimethoxyphenyl)-3-(3-(propylamino)propyl)thiourea hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether; water; for 0.25h;
DOI:10.1016/j.ejmech.2010.11.003

Reference yield:

: 7249-87-8
(3-isopropylamino)propanenitrile

: 1276682-54-2
1-(4-chloro-2,5-dimethoxyphenyl)-3-(3-(propylamino)propyl)thiourea hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydrogencarbonate / methanol / 6 h / Inert atmosphere; Sonication

2.1: dimethylsulfide borane complex / tetrahydrofuran / 4.5 h / 0 °C / Reflux

2.2: 0.25 h / 20 °C

3.1: triethylamine / chloroform / 20 °C

4.1: hydrogenchloride / diethyl ether; water / 0.25 h

With hydrogenchloride; dimethylsulfide borane complex; sodium hydrogencarbonate; triethylamine; In tetrahydrofuran; methanol; diethyl ether; chloroform; water;
DOI:10.1016/j.ejmech.2010.11.003

Reference yield:

: 1276682-56-4
tert-butyl 2-cyanoethylpropylcarbamate

: 1276682-54-2
1-(4-chloro-2,5-dimethoxyphenyl)-3-(3-(propylamino)propyl)thiourea hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 4.5 h / 0 °C / Reflux

1.2: 0.25 h / 20 °C

2.1: triethylamine / chloroform / 20 °C

3.1: hydrogenchloride / diethyl ether; water / 0.25 h

With hydrogenchloride; dimethylsulfide borane complex; triethylamine; In tetrahydrofuran; diethyl ether; chloroform; water;
DOI:10.1016/j.ejmech.2010.11.003