tert-butyl 3-(3-(4-chloro-2,5-dimethoxyphenyl)thioureido)propylpropylcarbamate

Base Information

Chemical Name:tert-butyl 3-(3-(4-chloro-2,5-dimethoxyphenyl)thioureido)propylpropylcarbamate
CAS No.:1159074-29-9
Molecular Formula:C₂₀H₃₂ClN₃O₄S
Molecular Weight:446.011
Hs Code.:

Synonyms:tert-butyl 3-(3-(4-chloro-2,5-dimethoxyphenyl)thioureido)propylpropylcarbamate

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Chemical Property of tert-butyl 3-(3-(4-chloro-2,5-dimethoxyphenyl)thioureido)propylpropylcarbamate

Chemical Property:

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Technology Process of tert-butyl 3-(3-(4-chloro-2,5-dimethoxyphenyl)thioureido)propylpropylcarbamate

There total 4 articles about tert-butyl 3-(3-(4-chloro-2,5-dimethoxyphenyl)thioureido)propylpropylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 306935-82-0
1-chloro-4-isothiocyanato-2,5-dimethoxybenzene

: (3-amino-propyl)-propyl-carbamic acid tert-butyl ester

: 1159074-29-9
tert-butyl 3-(3-(4-chloro-2,5-dimethoxyphenyl)thioureido)propylpropylcarbamate

Guidance literature:: With triethylamine; In chloroform; at 20 ℃;
DOI:10.1016/j.ejmech.2010.11.003

Reference yield:

: 1276682-56-4
tert-butyl 2-cyanoethylpropylcarbamate

: 1159074-29-9
tert-butyl 3-(3-(4-chloro-2,5-dimethoxyphenyl)thioureido)propylpropylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 4.5 h / 0 °C / Reflux

1.2: 0.25 h / 20 °C

2.1: triethylamine / chloroform / 20 °C

With dimethylsulfide borane complex; triethylamine; In tetrahydrofuran; chloroform;
DOI:10.1016/j.ejmech.2010.11.003

Reference yield:

: 6358-64-1
4-chloro-2,5-dimethoxy-aniline

: 1159074-29-9
tert-butyl 3-(3-(4-chloro-2,5-dimethoxyphenyl)thioureido)propylpropylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: chloroform / 4.5 h / Reflux

2: triethylamine / chloroform / 20 °C

With triethylamine; In chloroform;
DOI:10.1016/j.ejmech.2010.11.003