benzyl (4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-β-D-glucopyranoside)uronate

Base Information

Chemical Name:benzyl (4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-β-D-glucopyranoside)uronate
CAS No.:1436409-49-2
Molecular Formula:C₃₉H₃₈O₁₁
Molecular Weight:682.724
Hs Code.:

Synonyms:benzyl (4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-β-D-glucopyranoside)uronate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl (4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-β-D-glucopyranoside)uronate

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Technology Process of benzyl (4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-β-D-glucopyranoside)uronate

There total 3 articles about benzyl (4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-β-D-glucopyranoside)uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1436409-46-9
benzyl (4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-β-D-glucopyranoside)uronate

: 123-76-2
levulinic acid

: 1436409-49-2
benzyl (4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-β-D-glucopyranoside)uronate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 3h;
DOI:10.1039/c3ob40306h

Reference yield:

: 428865-77-4
4-methoxyphenyl 2-O-benzyol-3-O-benzyl-β-D-glucopyranoside

: 1436409-49-2
benzyl (4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-β-D-glucopyranoside)uronate

Guidance literature:: Multi-step reaction with 3 steps

1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutylammomium bromide; potassium bromide; calcium hypochlorite; sodium hydrogencarbonate / dichloromethane; water / 1 h / 0 °C

2: tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 3 h / 60 °C

3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 3 h

With dmap; calcium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutylammomium bromide; tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; potassium bromide; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/c3ob40306h

Reference yield:

: C₂₇H₂₆O₉

: 1436409-49-2
benzyl (4-methoxyphenyl 2-O-benzoyl-3-O-benzyl-4-O-levulinoyl-β-D-glucopyranoside)uronate

Guidance literature:: Multi-step reaction with 2 steps

1: tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 3 h / 60 °C

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 3 h

With dmap; tetra-(n-butyl)ammonium iodide; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3ob40306h