2-(3,5-di-tert-butyl-4-methoxy-2,6-dimethylphenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

Base Information

Chemical Name:2-(3,5-di-tert-butyl-4-methoxy-2,6-dimethylphenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane
CAS No.:1208459-63-5
Molecular Formula:C₂₃H₃₉BO₃
Molecular Weight:374.372
Hs Code.:

Synonyms:2-(3,5-di-tert-butyl-4-methoxy-2,6-dimethylphenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

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Chemical Property of 2-(3,5-di-tert-butyl-4-methoxy-2,6-dimethylphenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

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Technology Process of 2-(3,5-di-tert-butyl-4-methoxy-2,6-dimethylphenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

There total 1 articles about 2-(3,5-di-tert-butyl-4-methoxy-2,6-dimethylphenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1208459-46-4
2,6-di-tert-butyl-4-iodo-3,5-dimethylanisole

: 73183-34-3
bis(pinacol)diborane

: 1208459-37-3
2,6-di-tert-butyl-3,5-dimethylanisole

: 1208459-63-5
2-(3,5-di-tert-butyl-4-methoxy-2,6-dimethylphenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In dichloromethane; dimethyl sulfoxide; at 80 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.11.103

Reference yield:

: 1208459-63-5
2-(3,5-di-tert-butyl-4-methoxy-2,6-dimethylphenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

: 1208459-37-3
2,6-di-tert-butyl-3,5-dimethylanisole

Guidance literature:: 2-(3,5-di-tert-butyl-4-methoxy-2,6-dimethylphenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 3h; Inert atmosphere;

With Glauber's salt; sulfuric acid; In tetrahydrofuran; water;
DOI:10.1016/j.tet.2009.11.103