1-iodo-7α,8α-[N-(4-bromophenyl)-2,5-dioxopyrrolidino][3,4-h]-6,14-endo-etheno-6,7,8,14-tetrahydrothebaine

Base Information

Chemical Name:1-iodo-7α,8α-[N-(4-bromophenyl)-2,5-dioxopyrrolidino][3,4-h]-6,14-endo-etheno-6,7,8,14-tetrahydrothebaine
CAS No.:1416672-95-1
Molecular Formula:C₂₉H₂₆BrIN₂O₅
Molecular Weight:689.344
Hs Code.:

Synonyms:1-iodo-7α,8α-[N-(4-bromophenyl)-2,5-dioxopyrrolidino][3,4-h]-6,14-endo-etheno-6,7,8,14-tetrahydrothebaine

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Chemical Property of 1-iodo-7α,8α-[N-(4-bromophenyl)-2,5-dioxopyrrolidino][3,4-h]-6,14-endo-etheno-6,7,8,14-tetrahydrothebaine

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Technology Process of 1-iodo-7α,8α-[N-(4-bromophenyl)-2,5-dioxopyrrolidino][3,4-h]-6,14-endo-etheno-6,7,8,14-tetrahydrothebaine

There total 1 articles about 1-iodo-7α,8α-[N-(4-bromophenyl)-2,5-dioxopyrrolidino][3,4-h]-6,14-endo-etheno-6,7,8,14-tetrahydrothebaine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 766550-46-3
C₂₉H₂₇BrN₂O₅

: 1416672-95-1
1-iodo-7α,8α-[N-(4-bromophenyl)-2,5-dioxopyrrolidino][3,4-h]-6,14-endo-etheno-6,7,8,14-tetrahydrothebaine

Guidance literature:: With N-iodo-succinimide; trifluoroacetic acid; at 20 ℃; for 2h;
DOI:10.1134/S1070428012110103

Reference yield: 80.0%

: 1416672-95-1
1-iodo-7α,8α-[N-(4-bromophenyl)-2,5-dioxopyrrolidino][3,4-h]-6,14-endo-etheno-6,7,8,14-tetrahydrothebaine

: 1066-54-2
trimethylsilylacetylene

: 1416673-19-2
1-(2-trimethylsilylethynyl)-7α,8α-[N-(4-bromophenyl)-2,5-dioxopyrrolidino][3,4-h]-6,14-endo-etheno-6,7,8,14-tetrahydrothebaine

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine; In benzene; at 60 ℃; Inert atmosphere;
DOI:10.1134/S1070428012110103