Technology Process of C14H22N2O7
There total 1 articles about C14H22N2O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: pyridine / 12 h / 0 - 20 °C
2.1: trimethylaluminum / toluene; n-heptane / 0.5 h / 110 °C / Molecular sieve
2.2: 130 °C / Molecular sieve; Sealed tube
3.1: triethylamine; triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 45 h / 20 °C
With
pyridine; trimethylaluminum; triethylamine tris(hydrogen fluoride); triethylamine;
In
tetrahydrofuran; n-heptane; toluene;
DOI:10.1002/cmdc.201402099
- Guidance literature:
-
Multi-step reaction with 6 steps
1: pyridine / 20 °C / Cooling with ice
2: triethylamine / acetonitrile / 0.5 h / 20 °C / Inert atmosphere
3: trichlorophosphate / 1 h / 0 - 20 °C
4: ammonium hydroxide / 1,4-dioxane / 12 h / 20 °C
5: N,N-dimethyl-formamide / 12 h / 20 °C
6: 1H-tetrazole; 1-methyl-1H-imidazole / N,N-dimethyl-formamide / 20 °C
With
pyridine; 1-methyl-1H-imidazole; 1H-tetrazole; ammonium hydroxide; triethylamine; trichlorophosphate;
In
1,4-dioxane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/cmdc.201402099
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine / 20 °C / Cooling with ice
2: triethylamine / acetonitrile / 0.5 h / 20 °C / Inert atmosphere
With
pyridine; triethylamine;
In
acetonitrile;
DOI:10.1002/cmdc.201402099
