1,3,5,7-tetramethyl-2,6-diethyl-8-phenyl-4,4'-diethyl-bora-3a,4a-diaza-s-indacene

Base Information

Chemical Name:1,3,5,7-tetramethyl-2,6-diethyl-8-phenyl-4,4'-diethyl-bora-3a,4a-diaza-s-indacene
CAS No.:1355046-25-1
Molecular Formula:C₂₇H₃₇BN₂
Molecular Weight:400.415
Hs Code.:

Synonyms:1,3,5,7-tetramethyl-2,6-diethyl-8-phenyl-4,4'-diethyl-bora-3a,4a-diaza-s-indacene

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Chemical Property of 1,3,5,7-tetramethyl-2,6-diethyl-8-phenyl-4,4'-diethyl-bora-3a,4a-diaza-s-indacene

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Technology Process of 1,3,5,7-tetramethyl-2,6-diethyl-8-phenyl-4,4'-diethyl-bora-3a,4a-diaza-s-indacene

There total 3 articles about 1,3,5,7-tetramethyl-2,6-diethyl-8-phenyl-4,4'-diethyl-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1355046-09-1
1,3,5,7-tetramethyl-2,6-diethyl-8-phenyl-4,4'-dichloro-bora-3a,4a-diaza-s-indacene

: 925-90-6
ethylmagnesium bromide

: 1355046-25-1
1,3,5,7-tetramethyl-2,6-diethyl-8-phenyl-4,4'-diethyl-bora-3a,4a-diaza-s-indacene

Guidance literature:: In diethyl ether; at 22 ℃; for 3h;
DOI:10.1039/c1cc16351e

Reference yield: 80.0%

: 96-10-6
diethylaluminium chloride

: 2,6-diethyl-4,4-difluoro-1,3,5,7-tetramethyl-8-phenyl-4-bora-3a,4a-diaza-s-indecene

: 1355046-25-1
1,3,5,7-tetramethyl-2,6-diethyl-8-phenyl-4,4'-diethyl-bora-3a,4a-diaza-s-indacene

Guidance literature:: In hexane; dichloromethane; at 25 ℃; for 0.0833333h; chemoselective reaction;
DOI:10.1021/jo502028g

Reference yield:

: 2,6-diethyl-4,4-difluoro-1,3,5,7-tetramethyl-8-phenyl-4-bora-3a,4a-diaza-s-indecene

: 1355046-25-1
1,3,5,7-tetramethyl-2,6-diethyl-8-phenyl-4,4'-diethyl-bora-3a,4a-diaza-s-indacene

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane; hexane / 1 h

2: dichloromethane; hexane; diethyl ether / 1 h

In diethyl ether; hexane; dichloromethane;
DOI:10.1021/jo302277d