(2R,3R)-ethyl 1-(1-(2-chlorophenyl)-2-nitroethyl)-2-oxocyclopentanecarboxylate

Base Information

Chemical Name:(2R,3R)-ethyl 1-(1-(2-chlorophenyl)-2-nitroethyl)-2-oxocyclopentanecarboxylate
CAS No.:1357385-17-1
Molecular Formula:C₁₆H₁₈ClNO₅
Molecular Weight:339.776
Hs Code.:

Synonyms:(2R,3R)-ethyl 1-(1-(2-chlorophenyl)-2-nitroethyl)-2-oxocyclopentanecarboxylate

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Chemical Property of (2R,3R)-ethyl 1-(1-(2-chlorophenyl)-2-nitroethyl)-2-oxocyclopentanecarboxylate

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Technology Process of (2R,3R)-ethyl 1-(1-(2-chlorophenyl)-2-nitroethyl)-2-oxocyclopentanecarboxylate

There total 2 articles about (2R,3R)-ethyl 1-(1-(2-chlorophenyl)-2-nitroethyl)-2-oxocyclopentanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 22568-07-6,3156-34-1
1-chloro-2-(2-nitrovinyl)benzene

: 611-10-9
2-ethoxycarbonyl-1-cyclopentanone

: 1357385-17-1
(2R,3R)-ethyl 1-(1-(2-chlorophenyl)-2-nitroethyl)-2-oxocyclopentanecarboxylate

Guidance literature:: With 4-methyl-morpholine; C₅₁H₅₂N₄O₅S₂; cobalt acetylacetonate; In 1,2-dichloro-ethane; at 0 ℃; for 12h; stereoselective reaction;
DOI:10.1039/c8ob00773j

Reference yield: 92.0%

: 611-10-9
2-ethoxycarbonyl-1-cyclopentanone

: 22568-07-6
1-chloro-2-[(E)-2-nitrovinyl]benzene

: 1357385-17-1
(2R,3R)-ethyl 1-(1-(2-chlorophenyl)-2-nitroethyl)-2-oxocyclopentanecarboxylate

Guidance literature:: With (S)-(-)-α,α-di(2-naphthyl)-2-pyrrolidinemethanol; In Hexafluorobenzene; at 20 ℃; optical yield given as %ee; enantioselective reaction;
DOI:10.1039/c2cc17488j