Technology Process of C35H41Cl2N5O2
There total 9 articles about C35H41Cl2N5O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C13H15Cl2NO2*ClH;
With
diethyl cyanophosphonate; triethylamine;
In
dichloromethane;
at 20 ℃;
for 0.166667h;
C22H28N4O;
In
dichloromethane;
at 20 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: diethyl cyanophosphonate; triethylamine / dichloromethane / 18 h
2.1: hydrogenchloride / isopropyl alcohol / 66 h / 60 °C
2.2: 1 h
3.1: diethyl cyanophosphonate; triethylamine / dichloromethane / 0.17 h / 20 °C
3.2: 3 h / 20 °C
With
hydrogenchloride; diethyl cyanophosphonate; triethylamine;
In
dichloromethane; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 0.08 h / 90 - 100 °C
2.1: hydrogenchloride / diethyl ether
3.1: lithium hydroxide; water / methanol / 0.33 h / Heating / reflux
3.2: 0.08 h / Heating / reflux
4.1: diethyl cyanophosphonate; triethylamine / dichloromethane / 0.17 h / 20 °C
4.2: 3 h / 20 °C
With
hydrogenchloride; lithium hydroxide; diethyl cyanophosphonate; water; triethylamine;
In
methanol; diethyl ether; dichloromethane;