6-O-benzoyl-3-O-benzyl-D-glucose propylene dithioacetal

Base Information

Chemical Name:6-O-benzoyl-3-O-benzyl-D-glucose propylene dithioacetal
CAS No.:195315-83-4
Molecular Formula:C₂₃H₂₈O₆S₂
Molecular Weight:464.604
Hs Code.:

Synonyms:6-O-benzoyl-3-O-benzyl-D-glucose propylene dithioacetal

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Chemical Property of 6-O-benzoyl-3-O-benzyl-D-glucose propylene dithioacetal

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Technology Process of 6-O-benzoyl-3-O-benzyl-D-glucose propylene dithioacetal

There total 5 articles about 6-O-benzoyl-3-O-benzyl-D-glucose propylene dithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 109-80-8
1.3-propanedithiol

: 142657-25-8,142698-90-6
6-O-benzoyl-3-O-benzyl-α/β-D-glucopyranose

: 195315-83-4
6-O-benzoyl-3-O-benzyl-D-glucose propylene dithioacetal

Guidance literature:: With zinc(II) chloride; In acetonitrile; at 60 ℃; for 6.5h;
DOI:10.1248/cpb.45.1265

Reference yield:

: 22529-61-9
(1R)-1-((3aR,6S,6aR)-6-(benzyloxy)-2,2-dimethyltetrahydrofuro(2,3-d)(1,3)dioxol-5-yl)ethane-1,2-diol

: 195315-83-4
6-O-benzoyl-3-O-benzyl-D-glucose propylene dithioacetal

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / pyridine / CH₂Cl₂ / 1 h / 0 °C

2: 76 percent / 6 N aq. HCl / tetrahydrofuran / 5 h / Heating

3: 55 percent / ZnCl₂ / acetonitrile / 6.5 h / 60 °C

With pyridine; hydrogenchloride; zinc(II) chloride; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1248/cpb.45.1265

Reference yield:

: 18685-18-2
3-O-benzyl-1,2-5,6-O-diisopropylidene-α-D-glucofuranose

: 195315-83-4
6-O-benzoyl-3-O-benzyl-D-glucose propylene dithioacetal

Guidance literature:: Multi-step reaction with 4 steps

1: H₂SO₄ / methanol / 0.25 h / Ambient temperature

2: 93 percent / pyridine / CH₂Cl₂ / 1 h / 0 °C

3: 76 percent / 6 N aq. HCl / tetrahydrofuran / 5 h / Heating

4: 55 percent / ZnCl₂ / acetonitrile / 6.5 h / 60 °C

With pyridine; hydrogenchloride; sulfuric acid; zinc(II) chloride; In tetrahydrofuran; methanol; dichloromethane; acetonitrile;
DOI:10.1248/cpb.45.1265