N'-(6-chloro-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl)benzhydrazide

Base Information

• Chemical Name: N'-(6-chloro-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl)benzhydrazide
• CAS No.: 1318988-72-5
• Molecular Formula: C₁₆H₁₂ClN₃O₄S₃
• Molecular Weight: 441.94

Synonyms:N'-(6-chloro-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl)benzhydrazide

Chemical Property of N'-(6-chloro-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl)benzhydrazide

Chemical Property:

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Technology Process of N'-(6-chloro-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl)benzhydrazide

There total 2 articles about N'-(6-chloro-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl)benzhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

benzoic acid hydrazide (613-94-5) + chlorek kwasu 6-chloro-3-metylotio-1,1-diokso-1,4,2-benzoditiazyno-7-karboksylowego (156775-41-6) → N'-(6-chloro-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl)benzhydrazide (1318988-72-5)

Guidance literature:

In benzene; at 5 - 20 ℃;

DOI:10.3987/COM-11-12164

Reference yield:

6-chloro-3-(methylthio)-1,1-dioxo-1,4,2-benzodithiazine-7-carboxylic acid → N'-(6-chloro-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl)benzhydrazide (1318988-72-5)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride

2: benzene / 5 - 20 °C

With thionyl chloride; In benzene;

DOI:10.3987/COM-11-12164

Reference yield: 62.0%

N'-(6-chloro-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine-7-carbonyl)benzhydrazide (1318988-72-5) → 6-chloro-7-(5-phenyl-1,3,4-oxadiazol-2-yl)-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine (1318988-78-1)

Guidance literature:

With thionyl chloride; at 20 ℃; for 20h; Reflux;

DOI:10.3987/COM-11-12164

upstream raw materials:

benzoic acid hydrazide

chlorek kwasu 6-chloro-3-metylotio-1,1-diokso-1,4,2-benzoditiazyno-7-karboksylowego

Downstream raw materials:

6-chloro-7-(5-phenyl-1,3,4-thiadiazol-2-yl)-3-methylthio-1,1-dioxo-1,4,2-benzodithiazine

3-amino-6-chloro-7-(5-phenyl-1,3,4-oxadiazol-2-yl)-1,1-dioxo-1,4,2-benzodithiazine

3-amino-6-chloro-7-(5-phenyl-1,3,4-thiadiazol-2-yl)-1,1-dioxo-1,4,2-benzodithiazine

3-amino-2-[2-benzylthio-4-chloro-5-(5-phenyl-1,3,4-oxadiazol-2-yl)benzenesulfonyl]guanidine

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