(R)-methyl 3-((2-aminophenyl)(cyclohexyl)amino)-2-(4-methylphenylsulfonamido)propionate

Base Information

Chemical Name:(R)-methyl 3-((2-aminophenyl)(cyclohexyl)amino)-2-(4-methylphenylsulfonamido)propionate
CAS No.:1246926-42-0
Molecular Formula:C₂₃H₃₁N₃O₄S
Molecular Weight:445.583
Hs Code.:

Synonyms:(R)-methyl 3-((2-aminophenyl)(cyclohexyl)amino)-2-(4-methylphenylsulfonamido)propionate

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Chemical Property of (R)-methyl 3-((2-aminophenyl)(cyclohexyl)amino)-2-(4-methylphenylsulfonamido)propionate

Chemical Property:

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Technology Process of (R)-methyl 3-((2-aminophenyl)(cyclohexyl)amino)-2-(4-methylphenylsulfonamido)propionate

There total 1 articles about (R)-methyl 3-((2-aminophenyl)(cyclohexyl)amino)-2-(4-methylphenylsulfonamido)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1246926-41-9
(R)-methyl 3-((2-(tert-butoxycarbonylamino)phenyl)(cyclohexyl)amino)-2-(4-methylphenylsulfonamido)propionate

: 1246926-42-0
(R)-methyl 3-((2-aminophenyl)(cyclohexyl)amino)-2-(4-methylphenylsulfonamido)propionate

Guidance literature:: (R)-methyl 3-((2-(tert-butoxycarbonylamino)phenyl)(cyclohexyl)amino)-2-(4-methylphenylsulfonamido)propionate; With hydrogenchloride; In ethyl acetate; at 20 ℃; for 1h;

With sodium hydrogencarbonate; In water; ethyl acetate;

Reference yield: 71.0%

: 1246926-42-0
(R)-methyl 3-((2-aminophenyl)(cyclohexyl)amino)-2-(4-methylphenylsulfonamido)propionate

: 1246926-43-1
(R)-N-(1-cyclohexyl-4-oxo-2,3,4,5-tetrahydro-1H-benzo[b][1,4]diazepin-3-yl)-4-methylbenzenesulfonamide

Guidance literature:: In o-xylene; for 14h; Reflux;

Reference yield:

: 1246926-42-0
(R)-methyl 3-((2-aminophenyl)(cyclohexyl)amino)-2-(4-methylphenylsulfonamido)propionate

: (R)-(-)-1-tert-butylcarbonylmethyl-2-oxo-3-amino-5-cyclohexyl-1,3,4,5-tetrahydro-2H-1,5-benzodiazepine

Guidance literature:: Multi-step reaction with 2 steps

1: o-xylene / 14 h / Reflux

2: hydrogen bromide / 1 h / Reflux

With hydrogen bromide; In o-xylene;