(R)-N-(1-cyclohexyl-4-oxo-2,3,4,5-tetrahydro-1H-benzo[b][1,4]diazepin-3-yl)-4-methylbenzenesulfonamide

Base Information

• Chemical Name: (R)-N-(1-cyclohexyl-4-oxo-2,3,4,5-tetrahydro-1H-benzo[b][1,4]diazepin-3-yl)-4-methylbenzenesulfonamide
• CAS No.: 1246926-43-1
• Molecular Formula: C₂₂H₂₇N₃O₃S
• Molecular Weight: 413.541

Synonyms:(R)-N-(1-cyclohexyl-4-oxo-2,3,4,5-tetrahydro-1H-benzo[b][1,4]diazepin-3-yl)-4-methylbenzenesulfonamide

Chemical Property of (R)-N-(1-cyclohexyl-4-oxo-2,3,4,5-tetrahydro-1H-benzo[b][1,4]diazepin-3-yl)-4-methylbenzenesulfonamide

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Technology Process of (R)-N-(1-cyclohexyl-4-oxo-2,3,4,5-tetrahydro-1H-benzo[b][1,4]diazepin-3-yl)-4-methylbenzenesulfonamide

There total 6 articles about (R)-N-(1-cyclohexyl-4-oxo-2,3,4,5-tetrahydro-1H-benzo[b][1,4]diazepin-3-yl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

(R)-methyl 3-((2-(tert-butoxycarbonylamino)phenyl)(cyclohexyl)amino)-2-(2,2,2-trifluoroacetamido)propionate (1246926-39-5) → (R)-N-(1-cyclohexyl-4-oxo-2,3,4,5-tetrahydro-1H-benzo[b][1,4]diazepin-3-yl)-4-methylbenzenesulfonamide (1246926-43-1)

Guidance literature:

With hydrogenchloride; In water; toluene; at 50 ℃; for 1h;

Reference yield: 88.0%

(R)-benzyl 3-((2-(benzoyloxycarbonylamino)phenyl)(cyclohexyl)amino)-2-(2,2,2-trifluoroacetamide)propionate (1246926-30-6) → (R)-N-(1-cyclohexyl-4-oxo-2,3,4,5-tetrahydro-1H-benzo[b][1,4]diazepin-3-yl)-4-methylbenzenesulfonamide (1246926-43-1)

Guidance literature:

5%-palladium/activated carbon; In water; at 20 ℃; for 13h; Inert atmosphere;

Reference yield: 88.0%

→ (R)-N-(1-cyclohexyl-4-oxo-2,3,4,5-tetrahydro-1H-benzo[b][1,4]diazepin-3-yl)-4-methylbenzenesulfonamide (1246926-43-1)

Guidance literature:

upstream raw materials:

(R)-benzyl 3-((2-aminophenyl)(cyclohexyl)amino)-2-(2,2,2-trifluoroacetamido)propionate

(R)-methyl 3-((2-(tert-butoxycarbonylamino)phenyl)(cyclohexyl)amino)-2-(2,2,2-trifluoroacetamido)propionate

(R)-methyl 3-((2-(tert-butoxycarbonylamino)phenyl)(cyclohexyl)amino)-2-(4-methylphenylsulfonamido)propionate

(R)-methyl 3-((2-aminophenyl)(cyclohexyl)amino)-2-(4-methylphenylsulfonamido)propionate

Downstream raw materials:

(R)-N-(5-cyclohexyl-1-(3,3-dimethyl-2-oxobutyl)-2-oxo-2,3,4,5-tetrahydro-1H-benzo[b][1,4]diazepin-3-yl)-2,2,2-trifluoroacetamide

(R)-(-)-3-[3-(1-tert-butylcarbonylmethyl-2-oxo-5-cyclohexyl-1,3,4,5-tetrahydro-2H-1,5-benzodiazepin-3-yl]ureido]benzoic acid

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