1-(1',2,3,3',4,4',6-hepta-O-acetyl-6'-deoxysucrose-6'-yl)-4-(m-tolyl)-1,2,3-triazole

Base Information

Chemical Name:1-(1',2,3,3',4,4',6-hepta-O-acetyl-6'-deoxysucrose-6'-yl)-4-(m-tolyl)-1,2,3-triazole
CAS No.:1453262-68-4
Molecular Formula:C₃₅H₄₃N₃O₁₇
Molecular Weight:777.736
Hs Code.:

Synonyms:1-(1',2,3,3',4,4',6-hepta-O-acetyl-6'-deoxysucrose-6'-yl)-4-(m-tolyl)-1,2,3-triazole

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Chemical Property of 1-(1',2,3,3',4,4',6-hepta-O-acetyl-6'-deoxysucrose-6'-yl)-4-(m-tolyl)-1,2,3-triazole

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Technology Process of 1-(1',2,3,3',4,4',6-hepta-O-acetyl-6'-deoxysucrose-6'-yl)-4-(m-tolyl)-1,2,3-triazole

There total 6 articles about 1-(1',2,3,3',4,4',6-hepta-O-acetyl-6'-deoxysucrose-6'-yl)-4-(m-tolyl)-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.6%

: 766-82-5
1-ethynyl-3-methyl-benzene

: 56720-33-3
1′,2,3,3′,4,4′,6-hepta-O-acetyl-6′-azido-6′-deoxysucrose

: 1453262-68-4
1-(1',2,3,3',4,4',6-hepta-O-acetyl-6'-deoxysucrose-6'-yl)-4-(m-tolyl)-1,2,3-triazole

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 70 ℃; for 0.0833333h; Microwave irradiation;
DOI:10.1016/j.carres.2013.06.017

Reference yield:

: 82540-66-7
1',2,3,3',4,4',6-hepta-O-acetyl-6'-O-methanesulfonyl sucrose

: 1453262-68-4
1-(1',2,3,3',4,4',6-hepta-O-acetyl-6'-deoxysucrose-6'-yl)-4-(m-tolyl)-1,2,3-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 0.17 h / 120 °C / Microwave irradiation

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / tert-butyl alcohol; water / 0.08 h / 70 °C / Microwave irradiation

With sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.carres.2013.06.017

Reference yield:

: 30694-62-3
1,3,4'-tri-O-acetyl-β-D-fructofuranosyl 2,3,4,6-tetra-O-acetyl-α-D-glucopyranoside

: 1453262-68-4
1-(1',2,3,3',4,4',6-hepta-O-acetyl-6'-deoxysucrose-6'-yl)-4-(m-tolyl)-1,2,3-triazole

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; sodium azide; triethylamine / dichloromethane / 2.5 h / 0 - 20 °C

2: sodium azide / N,N-dimethyl-formamide / 0.17 h / 120 °C / Microwave irradiation

3: copper(ll) sulfate pentahydrate; sodium L-ascorbate / tert-butyl alcohol; water / 0.08 h / 70 °C / Microwave irradiation

With dmap; sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; triethylamine; In dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.carres.2013.06.017