(R)-3-[(E)-3-phenyl-2-propenoyl]-5-triphenylmethyloxymethyltetronic acid

Base Information

Chemical Name:(R)-3-[(E)-3-phenyl-2-propenoyl]-5-triphenylmethyloxymethyltetronic acid
CAS No.:369384-39-4
Molecular Formula:C₃₃H₂₆O₅
Molecular Weight:502.566
Hs Code.:

Synonyms:(R)-3-[(E)-3-phenyl-2-propenoyl]-5-triphenylmethyloxymethyltetronic acid

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Chemical Property of (R)-3-[(E)-3-phenyl-2-propenoyl]-5-triphenylmethyloxymethyltetronic acid

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Technology Process of (R)-3-[(E)-3-phenyl-2-propenoyl]-5-triphenylmethyloxymethyltetronic acid

There total 5 articles about (R)-3-[(E)-3-phenyl-2-propenoyl]-5-triphenylmethyloxymethyltetronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 369384-38-3
methyl (R)-2-[(E)-3-oxo-5-phenyl-4-pentenoyl]-oxy-3-triphenylmethyloxypropionate

: 369384-39-4
(R)-3-[(E)-3-phenyl-2-propenoyl]-5-triphenylmethyloxymethyltetronic acid

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 23 ℃;
DOI:10.1021/jm0100741

Reference yield:

: 16814-88-3
methyl (2R)-2-methoxy-3-(triphenylmethoxy)propanoate

: 369384-39-4
(R)-3-[(E)-3-phenyl-2-propenoyl]-5-triphenylmethyloxymethyltetronic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / silver trifluoroacetate / tetrahydrofuran / 5 h / 23 °C

2: 73 percent / tetrabutylammonium fluoride / tetrahydrofuran / 23 °C

With tetrabutyl ammonium fluoride; silver trifluoroacetate; In tetrahydrofuran;
DOI:10.1021/jm0100741

Reference yield:

: 140-10-3
(E)-3-phenylacrylic acid

: 369384-39-4
(R)-3-[(E)-3-phenyl-2-propenoyl]-5-triphenylmethyloxymethyltetronic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: magnesium ethoxide / tetrahydrofuran / 24 h / 23 °C

1.2: 53 percent / 1,1'-carbonyldiimidazole / tetrahydrofuran / 14.5 h / 23 °C

2.1: 68 percent / silver trifluoroacetate / tetrahydrofuran / 5 h / 23 °C

3.1: 73 percent / tetrabutylammonium fluoride / tetrahydrofuran / 23 °C

With tetrabutyl ammonium fluoride; silver trifluoroacetate; magnesium ethylate; In tetrahydrofuran;
DOI:10.1021/jm0100741