methyl (R)-2-[(E)-3-oxo-5-phenyl-4-pentenoyl]-oxy-3-triphenylmethyloxypropionate

Base Information

Chemical Name:methyl (R)-2-[(E)-3-oxo-5-phenyl-4-pentenoyl]-oxy-3-triphenylmethyloxypropionate
CAS No.:369384-38-3
Molecular Formula:C₃₄H₃₀O₆
Molecular Weight:534.609
Hs Code.:

Synonyms:methyl (R)-2-[(E)-3-oxo-5-phenyl-4-pentenoyl]-oxy-3-triphenylmethyloxypropionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (R)-2-[(E)-3-oxo-5-phenyl-4-pentenoyl]-oxy-3-triphenylmethyloxypropionate

Chemical Property:

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Technology Process of methyl (R)-2-[(E)-3-oxo-5-phenyl-4-pentenoyl]-oxy-3-triphenylmethyloxypropionate

There total 4 articles about methyl (R)-2-[(E)-3-oxo-5-phenyl-4-pentenoyl]-oxy-3-triphenylmethyloxypropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 16814-88-3
methyl (2R)-2-methoxy-3-(triphenylmethoxy)propanoate

: 112185-26-9
S-tert-butyl (E)-3-oxo-5-phenyl-4-pentenethioate

: 369384-38-3
methyl (R)-2-[(E)-3-oxo-5-phenyl-4-pentenoyl]-oxy-3-triphenylmethyloxypropionate

Guidance literature:: With silver trifluoroacetate; In tetrahydrofuran; at 23 ℃;
DOI:10.1016/S0040-4039(96)02029-1

Reference yield:

: 140-10-3
(E)-3-phenylacrylic acid

: 369384-38-3
methyl (R)-2-[(E)-3-oxo-5-phenyl-4-pentenoyl]-oxy-3-triphenylmethyloxypropionate

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium ethoxide / tetrahydrofuran / 24 h / 23 °C

1.2: 53 percent / 1,1'-carbonyldiimidazole / tetrahydrofuran / 14.5 h / 23 °C

2.1: 68 percent / silver trifluoroacetate / tetrahydrofuran / 5 h / 23 °C

With silver trifluoroacetate; magnesium ethylate; In tetrahydrofuran;
DOI:10.1021/jm0100741

Reference yield:

: 140-10-3
(E)-3-phenylacrylic acid

: 369384-38-3
methyl (R)-2-[(E)-3-oxo-5-phenyl-4-pentenoyl]-oxy-3-triphenylmethyloxypropionate

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / CDI / tetrahydrofuran / 23 °C

2: 68 percent / CF₃COOAg / tetrahydrofuran / 23 °C

With silver trifluoroacetate; 1,1'-carbonyldiimidazole; In tetrahydrofuran;
DOI:10.1016/S0040-4039(96)02029-1