(+/-)-(1S,3aR,4S,5R,7aS)-1-ethyl-3a,4,5,7a-tetrahydro-5-<(phenylthio)methyl>-4-indanmethanol

Base Information

Chemical Name:(+/-)-(1S,3aR,4S,5R,7aS)-1-ethyl-3a,4,5,7a-tetrahydro-5-<(phenylthio)methyl>-4-indanmethanol
CAS No.:95588-46-8
Molecular Formula:C₁₉H₂₆OS
Molecular Weight:302.481
Hs Code.:

Synonyms:(+/-)-(1S,3aR,4S,5R,7aS)-1-ethyl-3a,4,5,7a-tetrahydro-5-<(phenylthio)methyl>-4-indanmethanol

Suppliers and Price of (+/-)-(1S,3aR,4S,5R,7aS)-1-ethyl-3a,4,5,7a-tetrahydro-5-<(phenylthio)methyl>-4-indanmethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-(1S,3aR,4S,5R,7aS)-1-ethyl-3a,4,5,7a-tetrahydro-5-<(phenylthio)methyl>-4-indanmethanol

Chemical Property:

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Technology Process of (+/-)-(1S,3aR,4S,5R,7aS)-1-ethyl-3a,4,5,7a-tetrahydro-5-<(phenylthio)methyl>-4-indanmethanol

There total 15 articles about (+/-)-(1S,3aR,4S,5R,7aS)-1-ethyl-3a,4,5,7a-tetrahydro-5-<(phenylthio)methyl>-4-indanmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95532-30-2
(+/-)-methyl (1S,3aR,4S,5R,7aS)-1-ethyl-3a,4,5,7a-tetrahydro-5-<(phenylthio)methyl>-4-indancarboxylate

: 95588-46-8
(+/-)-(1S,3aR,4S,5R,7aS)-1-ethyl-3a,4,5,7a-tetrahydro-5-<(phenylthio)methyl>-4-indanmethanol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃; Yield given;
DOI:10.1021/ja00413a037

Reference yield:

: 81331-47-7,95671-28-6
(+/-)-(1S,3aR,4S,5R,7aS)-1-ethyl-3a,4,5,7a-tetrahydro-5-<(phenylthio)methyl>-4-indancarboxylic acid

: 95588-46-8
(+/-)-(1S,3aR,4S,5R,7aS)-1-ethyl-3a,4,5,7a-tetrahydro-5-<(phenylthio)methyl>-4-indanmethanol

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 0 °C

2: LiAlH₄ / diethyl ether / 0 °C

With lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1021/jo00209a017

Reference yield:

: 76566-89-7,88244-69-3,78216-75-8,91109-68-1
(+/-)-1α-Ethyl-5β-(hydroxymethyl)-3aβ,4,5,7aα-tetrahydroindan-4β-carboxylic Acid γ-Lactone

: 95588-46-8
(+/-)-(1S,3aR,4S,5R,7aS)-1-ethyl-3a,4,5,7a-tetrahydro-5-<(phenylthio)methyl>-4-indanmethanol

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylformamide / 3 h / 110 °C

2: diethyl ether / 0 °C

3: LiAlH₄ / diethyl ether / 0 °C

With lithium aluminium tetrahydride; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/jo00209a017