1-[(3,4,5-trimethoxyphenyl)methyl]-7,8-(methylenedioxy)-2,3,4,5-tetrhydro-1H-2-benzazepine

Base Information

Chemical Name:1-[(3,4,5-trimethoxyphenyl)methyl]-7,8-(methylenedioxy)-2,3,4,5-tetrhydro-1H-2-benzazepine
CAS No.:99281-99-9
Molecular Formula:C₂₁H₂₅NO₅
Molecular Weight:371.433
Hs Code.:

Synonyms:1-[(3,4,5-trimethoxyphenyl)methyl]-7,8-(methylenedioxy)-2,3,4,5-tetrhydro-1H-2-benzazepine

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Chemical Property of 1-[(3,4,5-trimethoxyphenyl)methyl]-7,8-(methylenedioxy)-2,3,4,5-tetrhydro-1H-2-benzazepine

Chemical Property:

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Technology Process of 1-[(3,4,5-trimethoxyphenyl)methyl]-7,8-(methylenedioxy)-2,3,4,5-tetrhydro-1H-2-benzazepine

There total 4 articles about 1-[(3,4,5-trimethoxyphenyl)methyl]-7,8-(methylenedioxy)-2,3,4,5-tetrhydro-1H-2-benzazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5-(3,4,5-Trimethoxy-benzyl)-8,9-dihydro-7H-1,3-dioxa-6-aza-cyclohepta[f]indene

: 99281-99-9
1-[(3,4,5-trimethoxyphenyl)methyl]-7,8-(methylenedioxy)-2,3,4,5-tetrhydro-1H-2-benzazepine

Guidance literature:: With borane-THF; In tetrahydrofuran; for 9h; Yield given; Heating;
DOI:10.1021/jm00152a003

Reference yield:

: 78498-59-6
3-<-3,4-(methylenedioxy)phenyl>-1-aminopropane

: 99281-99-9
1-[(3,4,5-trimethoxyphenyl)methyl]-7,8-(methylenedioxy)-2,3,4,5-tetrhydro-1H-2-benzazepine

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 72 h / Heating

2: POCl₃ / acetonitrile / 5 h / Heating

3: BH₃*THF / tetrahydrofuran / 9 h / Heating

With borane-THF; trichlorophosphate; In tetrahydrofuran; toluene; acetonitrile;
DOI:10.1021/jm00152a003

Reference yield:

: 951-82-6
3,4,5-trimethoxyphenyl acetic acid

: 99281-99-9
1-[(3,4,5-trimethoxyphenyl)methyl]-7,8-(methylenedioxy)-2,3,4,5-tetrhydro-1H-2-benzazepine

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 72 h / Heating

2: POCl₃ / acetonitrile / 5 h / Heating

3: BH₃*THF / tetrahydrofuran / 9 h / Heating

With borane-THF; trichlorophosphate; In tetrahydrofuran; toluene; acetonitrile;
DOI:10.1021/jm00152a003