N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-N-(4-methoxyphenyl)-9-fluorenylmethyloxycarbonylaminoacetamide

Base Information

Chemical Name:N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-N-(4-methoxyphenyl)-9-fluorenylmethyloxycarbonylaminoacetamide
CAS No.:1341219-67-7
Molecular Formula:C₃₈H₄₄N₂O₆Si
Molecular Weight:652.863
Hs Code.:

Synonyms:N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-N-(4-methoxyphenyl)-9-fluorenylmethyloxycarbonylaminoacetamide

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Chemical Property of N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-N-(4-methoxyphenyl)-9-fluorenylmethyloxycarbonylaminoacetamide

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Technology Process of N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-N-(4-methoxyphenyl)-9-fluorenylmethyloxycarbonylaminoacetamide

There total 5 articles about N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-N-(4-methoxyphenyl)-9-fluorenylmethyloxycarbonylaminoacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 29022-11-5
N-(fluoren-9-ylmethoxycarbonyl)glycine

: 1341219-49-5
N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-p-anisidine

: 1341219-67-7
N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-N-(4-methoxyphenyl)-9-fluorenylmethyloxycarbonylaminoacetamide

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1021/jo201495w

Reference yield:

: 129742-36-5
(4-((tert-butyldimethylsilyl)oxy)-2-methoxybenzaldehyde)

: 1341219-67-7
N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-N-(4-methoxyphenyl)-9-fluorenylmethyloxycarbonylaminoacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / dichloromethane / 0.17 h / 20 °C

2: sodium tris(acetoxy)borohydride / 0.33 h / 0 - 20 °C

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / 20 °C

With dmap; sodium tris(acetoxy)borohydride; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1021/jo201495w

Reference yield:

: C₂₁H₂₉NO₃Si

: 1341219-67-7
N-(4-tert-butyldimethylsiloxy-2-methoxybenzyl)-N-(4-methoxyphenyl)-9-fluorenylmethyloxycarbonylaminoacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tris(acetoxy)borohydride / 0.33 h / 0 - 20 °C

2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.5 h / 20 °C

With dmap; sodium tris(acetoxy)borohydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;
DOI:10.1021/jo201495w