Methoxy-acetic acid (Z)-(R)-1-benzyloxymethyl-4,4,4-trifluoro-but-2-enyl ester

Base Information

Chemical Name:Methoxy-acetic acid (Z)-(R)-1-benzyloxymethyl-4,4,4-trifluoro-but-2-enyl ester
CAS No.:185424-05-9
Molecular Formula:C₁₅H₁₇F₃O₄
Molecular Weight:318.293
Hs Code.:

Synonyms:Methoxy-acetic acid (Z)-(R)-1-benzyloxymethyl-4,4,4-trifluoro-but-2-enyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methoxy-acetic acid (Z)-(R)-1-benzyloxymethyl-4,4,4-trifluoro-but-2-enyl ester

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Technology Process of Methoxy-acetic acid (Z)-(R)-1-benzyloxymethyl-4,4,4-trifluoro-but-2-enyl ester

There total 1 articles about Methoxy-acetic acid (Z)-(R)-1-benzyloxymethyl-4,4,4-trifluoro-but-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 38870-89-2
Methoxyacetyl chloride

: (Z)-(R)-1-Benzyloxy-5,5,5-trifluoro-pent-3-en-2-ol

: 185424-05-9
Methoxy-acetic acid (Z)-(R)-1-benzyloxymethyl-4,4,4-trifluoro-but-2-enyl ester

Guidance literature:: With pyridine; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1021/jo961246i

Reference yield:

: 185424-05-9
Methoxy-acetic acid (Z)-(R)-1-benzyloxymethyl-4,4,4-trifluoro-but-2-enyl ester

: 185424-38-8
(E)-(2S,3S)-6-Benzyloxy-2-methoxy-3-trifluoromethyl-hex-4-en-1-ol

Guidance literature:: With lithium aluminium tetrahydride; n-butyllithium; chloro-trimethyl-silane; 1,1,1,3,3,3-hexamethyl-disilazane; Yield given. Multistep reaction; 1.) THF, hexane, -78 deg C, 30 min, then room temp., overnight, 2.) THF, room temp., 2 h;
DOI:10.1021/jo961246i