acetic acid 3-(2,4-dichlorophenyl)-2-(2,4-dichlorophenylazo)-2-methylpropyl ester

Base Information

Chemical Name:acetic acid 3-(2,4-dichlorophenyl)-2-(2,4-dichlorophenylazo)-2-methylpropyl ester
CAS No.:1373396-03-2
Molecular Formula:C₁₈H₁₆Cl₄N₂O₂
Molecular Weight:434.149
Hs Code.:

Synonyms:acetic acid 3-(2,4-dichlorophenyl)-2-(2,4-dichlorophenylazo)-2-methylpropyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of acetic acid 3-(2,4-dichlorophenyl)-2-(2,4-dichlorophenylazo)-2-methylpropyl ester

Chemical Property:

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Technology Process of acetic acid 3-(2,4-dichlorophenyl)-2-(2,4-dichlorophenylazo)-2-methylpropyl ester

There total 1 articles about acetic acid 3-(2,4-dichlorophenyl)-2-(2,4-dichlorophenylazo)-2-methylpropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 820-71-3
methallyl acetate

: 21872-70-8
2,4-dichlorobenzenediazonium tetrafluoroborate

: 1373396-03-2
acetic acid 3-(2,4-dichlorophenyl)-2-(2,4-dichlorophenylazo)-2-methylpropyl ester

Guidance literature:: With ferrous(II) sulfate heptahydrate; In water; dimethyl sulfoxide; for 0.25h; Inert atmosphere;
DOI:10.1039/c2ob25247c

Reference yield:

: 1373396-03-2
acetic acid 3-(2,4-dichlorophenyl)-2-(2,4-dichlorophenylazo)-2-methylpropyl ester

: 1373396-39-4
3-(2,4-dichlorophenyl)-2-(2,4-dichlorophenylazo)-2-methylpropan-1-ol

: (R)-acetic acid 3-(2,4-dichlorophenyl)-2-(2,4-dichlorophenylazo)-2-methylpropyl ester

: 1373396-25-8
(S)-acetic acid 3-(2,4-dichlorophenyl)-2-(2,4-dichlorophenylazo)-2-methylpropyl ester

Guidance literature:: With Candida antarctica lipase B; benzylamine; In acetonitrile; at 20 ℃; for 39h; optical yield given as %ee; Enzymatic reaction;
DOI:10.1039/c2ob25247c

Reference yield:

: 1373396-03-2
acetic acid 3-(2,4-dichlorophenyl)-2-(2,4-dichlorophenylazo)-2-methylpropyl ester

: (R)-phthalic acid [3-(2,4-dichlorophenyl)-2-(2,4-dichlorophenylazo)-2-methylpropyl]ester

: 1373396-41-8
(S)-phthalic acid [3-(2,4-dichlorophenyl)-2-(2,4-dichlorophenylazo)-2-methylpropyl]ester

Guidance literature:: Multi-step reaction with 2 steps

1: Candida antarctica lipase B; benzylamine / acetonitrile / 39 h / 20 °C / Enzymatic reaction

2: triethylamine / dichloromethane / 2 h / 20 °C

With Candida antarctica lipase B; triethylamine; benzylamine; In dichloromethane; acetonitrile;
DOI:10.1039/c2ob25247c