(R)-1-(5-methyltetrahydrofuran-2-yl)propylamine para-toluenesulfonate salt

Base Information

Chemical Name:(R)-1-(5-methyltetrahydrofuran-2-yl)propylamine para-toluenesulfonate salt
CAS No.:1092389-28-0
Molecular Formula:C₇H₈O₃S*C₈H₁₇NO
Molecular Weight:315.434
Hs Code.:

Synonyms:(R)-1-(5-methyltetrahydrofuran-2-yl)propylamine para-toluenesulfonate salt

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Chemical Property of (R)-1-(5-methyltetrahydrofuran-2-yl)propylamine para-toluenesulfonate salt

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Technology Process of (R)-1-(5-methyltetrahydrofuran-2-yl)propylamine para-toluenesulfonate salt

There total 6 articles about (R)-1-(5-methyltetrahydrofuran-2-yl)propylamine para-toluenesulfonate salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (R)-1-(5-methylfuran-2-yl)propylamine para-toluenesulfonate

: 1092389-28-0
(R)-1-(5-methyltetrahydrofuran-2-yl)propylamine para-toluenesulfonate salt

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In methanol; at 20 ℃; under 262.526 Torr;

Reference yield:

: 779340-42-0
(R)-2-{[1-(5-methylfuran-2-yl)-(E)-methylidene]amino}-2-phenylethanol

: 1092389-28-0
(R)-1-(5-methyltetrahydrofuran-2-yl)propylamine para-toluenesulfonate salt

Guidance literature:: Multi-step reaction with 5 steps

1.1: ammonium sulfate / tetrahydrofuran / Heating / reflux

2.1: diethyl ether / 0.5 h / 22 - 35 °C

3.1: sulfuric acid / tert-butyl methyl ether; water / 0.5 h / 5 - 10 °C

3.2: pH 11

4.1: sodium peroxide; methylamine / ethanol; water / 3 h / 5 - 20 °C

4.2: 1 h / 0 - 20 °C

5.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C / 262.53 Torr

With sodium peroxide; ammonium sulfate; sulfuric acid; hydrogen; methylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; diethyl ether; ethanol; tert-butyl methyl ether; water;

Reference yield:

: 779340-43-1
[1-(5-methylfuran-2-yl)-(E)-methylidene]-((R)-1-phenyl-2-trimethylsilanyloxyethyl)amine

: 1092389-28-0
(R)-1-(5-methyltetrahydrofuran-2-yl)propylamine para-toluenesulfonate salt

Guidance literature:: Multi-step reaction with 4 steps

1.1: diethyl ether / 0.5 h / 22 - 35 °C

2.1: sulfuric acid / tert-butyl methyl ether; water / 0.5 h / 5 - 10 °C

2.2: pH 11

3.1: sodium peroxide; methylamine / ethanol; water / 3 h / 5 - 20 °C

3.2: 1 h / 0 - 20 °C

4.1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C / 262.53 Torr

With sodium peroxide; sulfuric acid; hydrogen; methylamine; palladium 10% on activated carbon; In methanol; diethyl ether; ethanol; tert-butyl methyl ether; water;