2-(2-N,N-diethylcarbamoyl-6-methoxyphenyl)-3-hydroxy-5-methoxy-1,4-naphthoquinone

Base Information

Chemical Name:2-(2-N,N-diethylcarbamoyl-6-methoxyphenyl)-3-hydroxy-5-methoxy-1,4-naphthoquinone
CAS No.:122775-52-4
Molecular Formula:C₂₃H₂₃NO₆
Molecular Weight:409.439
Hs Code.:

Synonyms:2-(2-N,N-diethylcarbamoyl-6-methoxyphenyl)-3-hydroxy-5-methoxy-1,4-naphthoquinone

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Chemical Property of 2-(2-N,N-diethylcarbamoyl-6-methoxyphenyl)-3-hydroxy-5-methoxy-1,4-naphthoquinone

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Technology Process of 2-(2-N,N-diethylcarbamoyl-6-methoxyphenyl)-3-hydroxy-5-methoxy-1,4-naphthoquinone

There total 4 articles about 2-(2-N,N-diethylcarbamoyl-6-methoxyphenyl)-3-hydroxy-5-methoxy-1,4-naphthoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 122775-49-9
2-(2-N,N-diethylcarbamoyl-6-methoxyphenyl)-5-methoxy-1,3-naphthalenediol

: 122775-52-4
2-(2-N,N-diethylcarbamoyl-6-methoxyphenyl)-3-hydroxy-5-methoxy-1,4-naphthoquinone

Guidance literature:: With air; In sodium hydroxide; ethanol; for 24h; Ambient temperature;
DOI:10.1248/cpb.37.292

Reference yield:

: 121425-20-5
N,N-diethyl-3-methoxy-2-methylbenzamide

: 122775-52-4
2-(2-N,N-diethylcarbamoyl-6-methoxyphenyl)-3-hydroxy-5-methoxy-1,4-naphthoquinone

Guidance literature:: Multi-step reaction with 4 steps

1: LDA / tetrahydrofuran; hexane / Ambient temperature

2: diethyl ether

3: 63 percent / NaOMe / methanol / 18 h / Heating

4: 97 percent / air / ethanol; aq. NaOH / 24 h / Ambient temperature

With air; sodium methylate; lithium diisopropyl amide; In tetrahydrofuran; methanol; sodium hydroxide; diethyl ether; ethanol; hexane;
DOI:10.1248/cpb.37.292

Reference yield:

: {2-[2-(2-Diethylcarbamoyl-6-methoxy-phenyl)-acetyl]-6-methoxy-phenyl}-acetic acid

: 122775-52-4
2-(2-N,N-diethylcarbamoyl-6-methoxyphenyl)-3-hydroxy-5-methoxy-1,4-naphthoquinone

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether

2: 63 percent / NaOMe / methanol / 18 h / Heating

3: 97 percent / air / ethanol; aq. NaOH / 24 h / Ambient temperature

With air; sodium methylate; In methanol; sodium hydroxide; diethyl ether; ethanol;
DOI:10.1248/cpb.37.292