3-<<(4-Methoxyphenyl)imino>methyl>-1-methylpyridinium-iodid-N-oxid

Base Information

• Chemical Name: 3-<<(4-Methoxyphenyl)imino>methyl>-1-methylpyridinium-iodid-N-oxid
• CAS No.: 97369-64-7
• Molecular Formula: C₁₄H₁₅N₂O₂*I
• Molecular Weight: 370.19
• Mol file: 97369-64-7.mol

Synonyms:3-<<(4-Methoxyphenyl)imino>methyl>-1-methylpyridinium-iodid-N-oxid

Chemical Property of 3-<<(4-Methoxyphenyl)imino>methyl>-1-methylpyridinium-iodid-N-oxid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-<<(4-Methoxyphenyl)imino>methyl>-1-methylpyridinium-iodid-N-oxid

There total 4 articles about 3-<<(4-Methoxyphenyl)imino>methyl>-1-methylpyridinium-iodid-N-oxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

C13H12N2O2 + methyl iodide (74-88-4) → 3-<<(4-Methoxyphenyl)imino>methyl>-1-methylpyridinium-iodid-N-oxid (97369-64-7)

Guidance literature:

In dichloromethane; at 20 ℃; under 760.051 Torr;

DOI:10.1021/acs.orglett.9b01863

Reference yield:

para-methoxynitrobenzene (100-17-4) → 3-<<(4-Methoxyphenyl)imino>methyl>-1-methylpyridinium-iodid-N-oxid (97369-64-7)

Guidance literature:

Multi-step reaction with 3 steps

1: ammonium chloride; zinc; water / ethanol / 0.5 h / 20 °C / 760.05 Torr

2: magnesium sulfate / dichloromethane / 18 h / 20 °C / 760.05 Torr

3: dichloromethane / 20 °C / 760.05 Torr

With water; magnesium sulfate; ammonium chloride; zinc; In ethanol; dichloromethane;

DOI:10.1021/acs.orglett.9b01863

Reference yield:

p-methoxyphenylhydroxylamine (4546-20-7) → 3-<<(4-Methoxyphenyl)imino>methyl>-1-methylpyridinium-iodid-N-oxid (97369-64-7)

Guidance literature:

Multi-step reaction with 2 steps

1: magnesium sulfate / dichloromethane / 18 h / 20 °C / 760.05 Torr

2: dichloromethane / 20 °C / 760.05 Torr

With magnesium sulfate; In dichloromethane;

DOI:10.1021/acs.orglett.9b01863

upstream raw materials:

p-methoxyphenylhydroxylamine

3-formylpyridinium methiodide

para-methoxynitrobenzene

methyl iodide