2-Methylbenzenecarbothioamide

Base Information

Chemical Name:2-Methylbenzenecarbothioamide
CAS No.:53515-19-8
Molecular Formula:C8H9NS
Molecular Weight:151.232
Hs Code.:2930909899
European Community (EC) Number:674-606-4
DSSTox Substance ID:DTXSID00355709
Nikkaji Number:J2.595.577C
Mol file:53515-19-8.mol

Synonyms:53515-19-8;2-Methylbenzenecarbothioamide;2-methylbenzothioamide;2-Methylthiobenzamide;2-Methyl-thiobenzamide;2-methylbenzene-1-carbothioamide;MFCD03945350;thiuram toluene;methyl-thiobenzamide;2-METHYLBENZTHIOAMIDE;2-Methylbenzenecarbothioamide #;SCHEMBL1379361;?2-METHYL-THIOBENZAMIDE;SCHEMBL18697895;DTXSID00355709;STK399876;AKOS000200490;AB16881;CS-W018110;FS-1643;FT-0704501;EN300-11449;A829645;AB-131/41020567;Z57046956;F1967-1440

Suppliers and Price of 2-Methylbenzenecarbothioamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Methylbenzenecarbothioamide
100mg
$ 75.00

Crysdot
2-Methylbenzothioamide 95+%
500g
$ 867.00

Chemenu
2-Methylbenzothioamide 95%
500g
$ 811.00

ChemBridge Corporation
2-methylbenzenecarbothioamide 95%
25 g
$ 178.40

Apolloscientific
2-Methylthiobenzamide 98%
100g
$ 435.00

Apolloscientific
2-Methylthiobenzamide 98%
25g
$ 167.00

Anichem
2-Methyl-thiobenzamide >95%
5g
$ 165.00

Anichem
2-Methyl-thiobenzamide >95%
50g
$ 500.00

Anichem
2-Methyl-thiobenzamide >95%
1g
$ 45.00

American Custom Chemicals Corporation
2-METHYL-THIOBENZAMIDE 95.00%
5G
$ 830.74

Total 14 raw suppliers

Chemical Property of 2-Methylbenzenecarbothioamide

Chemical Property:

Appearance/Colour:Powder
Vapor Pressure:0.00887mmHg at 25°C
Melting Point:142 °C
Refractive Index:1.633
Boiling Point:266 °C at 760 mmHg
Flash Point:114.7 °C
PSA：58.11000
Density:1.143 g/cm₃
LogP:2.32950
XLogP3:1.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:151.04557046
Heavy Atom Count:10
Complexity:133

Purity/Quality:

98%min ^*data from raw suppliers

2-Methylbenzenecarbothioamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Statements: 36/37/38
Safety Statements: 26-36/37/39

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=CC=C1C(=S)N

Technology Process of 2-Methylbenzenecarbothioamide

There total 5 articles about 2-Methylbenzenecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 529-19-1
2-Methylbenzonitrile

: 53515-19-8
2-methylthiobenzamide

Guidance literature:: 2-Methylbenzonitrile; With calcium hydride; tiolacetic acid; at 80 ℃; for 1.25h;

With water; In ethyl acetate; at 20 ℃;
DOI:10.1055/s-0029-1217711

Reference yield: 68.0%

: 527-85-5
o-Methylbenzamid

: 53515-19-8
2-methylthiobenzamide

Guidance literature:: With P₂S₅/alumina; In tetrahydrofuran; at 60 ℃; for 0.333333h; Microwave irradiation;
DOI:10.1002/chem.201301011

Reference yield:

: 118-90-1
ortho-methylbenzoic acid

: 53515-19-8
2-methylthiobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / chloroform / 8 h / Reflux

2: ammonium hydroxide / tetrahydrofuran / 2 h / 20 °C

3: Lawessons reagent / tetrahydrofuran / Reflux

With Lawessons reagent; ammonium hydroxide; thionyl chloride; In tetrahydrofuran; chloroform;
DOI:10.1016/j.bmcl.2012.12.065