dimethyl (2E,4Z)-4-{[(2,6-dichlorophenyl)amino]methylene}-2-pentenedioate

Base Information

Chemical Name:dimethyl (2E,4Z)-4-{[(2,6-dichlorophenyl)amino]methylene}-2-pentenedioate
CAS No.:1082295-38-2
Molecular Formula:C₁₄H₁₃Cl₂NO₄
Molecular Weight:330.168
Hs Code.:

Synonyms:dimethyl (2E,4Z)-4-{[(2,6-dichlorophenyl)amino]methylene}-2-pentenedioate

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Chemical Property of dimethyl (2E,4Z)-4-{[(2,6-dichlorophenyl)amino]methylene}-2-pentenedioate

Chemical Property:

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Technology Process of dimethyl (2E,4Z)-4-{[(2,6-dichlorophenyl)amino]methylene}-2-pentenedioate

There total 1 articles about dimethyl (2E,4Z)-4-{[(2,6-dichlorophenyl)amino]methylene}-2-pentenedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 114106-77-3
methyl 4-carbomethoxy-5-methoxy-penta-2(E),4(Z)-dienoate

: 608-31-1
2,6-Dichloroaniline

: 1082295-38-2
dimethyl (2E,4Z)-4-{[(2,6-dichlorophenyl)amino]methylene}-2-pentenedioate

Guidance literature:: 2,6-Dichloroaniline; With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; for 0.5h;

methyl 4-carbomethoxy-5-methoxy-penta-2(E),4(Z)-dienoate; In tetrahydrofuran; at 0 ℃; for 3h;

Reference yield:

: 1082295-38-2
dimethyl (2E,4Z)-4-{[(2,6-dichlorophenyl)amino]methylene}-2-pentenedioate

: 1082295-56-4
methyl 1-(2,6-dichlorophenyl)-6-oxo-1,6-dihydro-3-pyridinecarboxylate

Guidance literature:: With sodium methylate; In methanol; for 8h; Heating / reflux;

Reference yield:

: 1082295-38-2
dimethyl (2E,4Z)-4-{[(2,6-dichlorophenyl)amino]methylene}-2-pentenedioate

: 1082295-91-7
4-chloro-3-({[1-(2,6-dichlorophenyl)-6-oxo-1,6-dihydro-3-pyridinyl]carbonyl}amino)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 8 h / Heating / reflux

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.25 h / -10 - -5 °C

2.2: 3 h / -10 °C

With sodium methylate; lithium hexamethyldisilazane; In tetrahydrofuran; methanol;