(S)-2-((R)-2-tert-Butoxycarbonylamino-4-carbamoyl-butyrylamino)-pentanedioic acid dibenzyl ester

Base Information

Chemical Name:(S)-2-((R)-2-tert-Butoxycarbonylamino-4-carbamoyl-butyrylamino)-pentanedioic acid dibenzyl ester
CAS No.:499775-49-4
Molecular Formula:C₂₉H₃₇N₃O₈
Molecular Weight:555.628
Hs Code.:

Synonyms:(S)-2-((R)-2-tert-Butoxycarbonylamino-4-carbamoyl-butyrylamino)-pentanedioic acid dibenzyl ester

Suppliers and Price of (S)-2-((R)-2-tert-Butoxycarbonylamino-4-carbamoyl-butyrylamino)-pentanedioic acid dibenzyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (S)-2-((R)-2-tert-Butoxycarbonylamino-4-carbamoyl-butyrylamino)-pentanedioic acid dibenzyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (S)-2-((R)-2-tert-Butoxycarbonylamino-4-carbamoyl-butyrylamino)-pentanedioic acid dibenzyl ester

There total 1 articles about (S)-2-((R)-2-tert-Butoxycarbonylamino-4-carbamoyl-butyrylamino)-pentanedioic acid dibenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 61348-28-5
(2R)-5-amino-2-(tert-butoxycarbonylamino)-5-oxo-pentanoic acid

: (S)-2-Amino-pentanedioic acid dibenzyl ester; compound with trifluoro-acetic acid

: 499775-49-4
(S)-2-((R)-2-tert-Butoxycarbonylamino-4-carbamoyl-butyrylamino)-pentanedioic acid dibenzyl ester

Guidance literature:: With 4-methyl-morpholine; isobutyl chloroformate; In N,N-dimethyl-formamide; at -10 ℃; for 2h;
DOI:10.1016/S0040-4020(02)01021-9

Reference yield:

: 499775-49-4
(S)-2-((R)-2-tert-Butoxycarbonylamino-4-carbamoyl-butyrylamino)-pentanedioic acid dibenzyl ester

: 499775-24-5
[(2S,5R)-5-(2-Benzyloxycarbonylamino-ethyl)-3,6-dioxo-piperazin-2-yl]-acetic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / dimethylformamide; H₂O / 3 h

2: 93 percent / N-methylmorpholine / acetonitrile / 0 - 20 °C

3: acetic acid / 2 h / 20 °C

4: N-methylmorpholine; acetic acid / butan-2-ol / Heating

With 4-methyl-morpholine; pyridine; acetic acid; In water; N,N-dimethyl-formamide; acetonitrile; iso-butanol;
DOI:10.1016/S0040-4020(02)01021-9

Reference yield:

: 499775-49-4
(S)-2-((R)-2-tert-Butoxycarbonylamino-4-carbamoyl-butyrylamino)-pentanedioic acid dibenzyl ester

: 499775-45-0
(S)-2-((R)-4-Benzyloxycarbonylamino-2-tert-butoxycarbonylamino-butyrylamino)-succinic acid dibenzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dimethylformamide; H₂O / 3 h

2: 93 percent / N-methylmorpholine / acetonitrile / 0 - 20 °C

With 4-methyl-morpholine; pyridine; In water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4020(02)01021-9