2-Piperazineacetic acid, 5-(2-aminoethyl)-3,6-dioxo-, (2S,5R)- (9CI)

Base Information

• Chemical Name: 2-Piperazineacetic acid, 5-(2-aminoethyl)-3,6-dioxo-, (2S,5R)- (9CI)
• CAS No.: 499775-01-8
• Molecular Formula: C₈H₁₃N₃O₄
• Molecular Weight: 215.209
• Mol file: 499775-01-8.mol

Synonyms:2-Piperazineacetic acid, 5-(2-aminoethyl)-3,6-dioxo-, (2S,5R)- (9CI)

Chemical Property of 2-Piperazineacetic acid, 5-(2-aminoethyl)-3,6-dioxo-, (2S,5R)- (9CI)

Chemical Property:

• PSA: 0.00000
• LogP: 0.00000

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 2-Piperazineacetic acid, 5-(2-aminoethyl)-3,6-dioxo-, (2S,5R)- (9CI)

There total 17 articles about 2-Piperazineacetic acid, 5-(2-aminoethyl)-3,6-dioxo-, (2S,5R)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

[(2S,5S)-5-(2-Benzyloxycarbonylamino-ethyl)-3,6-dioxo-piperazin-2-yl]-acetic acid benzyl ester (499775-20-1) → [(2S,5S)-5-(2-Amino-ethyl)-3,6-dioxo-piperazin-2-yl]-acetic acid (499775-01-8)

Guidance literature:

With formic acid; acetic acid; palladium oxide on charcoal; In isopropyl alcohol;

DOI:10.1016/S0040-4020(02)01021-9

Reference yield: 60.0%

[(2R,5S)-5-(2-Benzyloxycarbonylamino-ethyl)-3,6-dioxo-piperazin-2-yl]-acetic acid benzyl ester (499775-21-2) → [(2R,5S)-5-(2-Amino-ethyl)-3,6-dioxo-piperazin-2-yl]-acetic acid (499775-01-8)

Guidance literature:

With formic acid; acetic acid; palladium oxide on charcoal; In isopropyl alcohol;

DOI:10.1016/S0040-4020(02)01021-9

Reference yield: 52.0%

[(2R,5R)-5-(2-Benzyloxycarbonylamino-ethyl)-3,6-dioxo-piperazin-2-yl]-acetic acid benzyl ester (499775-25-6) → [(2R,5R)-5-(2-Amino-ethyl)-3,6-dioxo-piperazin-2-yl]-acetic acid (499775-01-8)

Guidance literature:

With formic acid; acetic acid; palladium oxide on charcoal; In isopropyl alcohol;

DOI:10.1016/S0040-4020(02)01021-9

upstream raw materials:

[(2S,5R)-5-(2-Benzyloxycarbonylamino-ethyl)-3,6-dioxo-piperazin-2-yl]-acetic acid benzyl ester

(S)-2-((R)-2-tert-Butoxycarbonylamino-4-carbamoyl-butyrylamino)-pentanedioic acid dibenzyl ester

(S)-2-((R)-4-Benzyloxycarbonylamino-2-tert-butoxycarbonylamino-butyrylamino)-succinic acid dibenzyl ester

[(2S,5S)-5-(2-Benzyloxycarbonylamino-ethyl)-3,6-dioxo-piperazin-2-yl]-acetic acid benzyl ester

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