Technology Process of C16H22N4O
There total 5 articles about C16H22N4O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium 10% on activated carbon;
In
methanol;
at 20 ℃;
for 48h;
under 760.051 Torr;
Inert atmosphere of argon;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 / tetrahydrofuran; water / 1.5 h / 80 °C
2.1: methanesulfonyl chloride; triethylamine / tetrahydrofuran / 0 - 20 °C
2.2: 87 h / 50 - 60 °C
3.1: hydrogen / palladium 10% on activated carbon / methanol / 48 h / 20 °C / 760.05 Torr / Inert atmosphere of argon
With
hydrogen; sodium carbonate; methanesulfonyl chloride; triethylamine;
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; water;
1.1: Suzuki Coupling;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: methanesulfonyl chloride; triethylamine / tetrahydrofuran / 0 - 20 °C
1.2: 87 h / 50 - 60 °C
2.1: hydrogen / palladium 10% on activated carbon / methanol / 48 h / 20 °C / 760.05 Torr / Inert atmosphere of argon
With
hydrogen; methanesulfonyl chloride; triethylamine;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol;