(S)-oxy>-1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>amino>acetic acid phenylmethyl ester

Base Information

Chemical Name:(S)-oxy>-1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>amino>acetic acid phenylmethyl ester
CAS No.:126110-76-7
Molecular Formula:C₃₉H₅₁N₂O₈P
Molecular Weight:706.816
Hs Code.:

(S)-<cyclohexyl<2-<<hydroxy(4-phenylbutyl)phosphinyl>oxy>-1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>amino>acetic acid phenylmethyl ester

Synonyms:(S)-oxy>-1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>amino>acetic acid phenylmethyl ester

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Chemical Property of (S)-oxy>-1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>amino>acetic acid phenylmethyl ester

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Technology Process of (S)-oxy>-1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>amino>acetic acid phenylmethyl ester

There total 6 articles about (S)-oxy>-1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>amino>acetic acid phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 126111-00-0
(cyclohexylamino)acetic acid phenylmethyl ester monohydrochloride

: 107492-16-0
(S)-2-<oxy>-6-<<(phenylmethoxy)carbonyl>amino>hexanoic acid

: 126110-76-7
(S)-oxy>-1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>amino>acetic acid phenylmethyl ester

Guidance literature:: With triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; for 6h; Ambient temperature;
DOI:10.1021/jm00167a028

Reference yield:

: 86552-32-1
(4-phenylbutyl)phosphinic acid

: 126110-76-7
(S)-oxy>-1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>amino>acetic acid phenylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 5.77 g / N,N'-dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / tetrahydrofuran / 0.67 h / Ambient temperature

2: NaIO₄ / dioxane; H₂O / 16 h / Ambient temperature

3: 99 percent / 2.0 N NaOH / dioxane / 2 h / Ambient temperature

4: 52 percent / triethylamine, N,N'-dicyclohexylcarbodiimide / tetrahydrofuran / 6 h / Ambient temperature

With dmap; sodium hydroxide; sodium periodate; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1021/jm00167a028

Reference yield:

: 59221-35-1
(S)-6-[[(Phenylmethoxy)carbonyl]amino]-2-hydroxyhexanoic acid

: 126110-76-7
(S)-oxy>-1-oxo-6-<<(phenylmethoxy)carbonyl>amino>hexyl>amino>acetic acid phenylmethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / potassium carbonate / dimethylformamide / 2 h / Ambient temperature

2: 5.77 g / N,N'-dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / tetrahydrofuran / 0.67 h / Ambient temperature

3: NaIO₄ / dioxane; H₂O / 16 h / Ambient temperature

4: 99 percent / 2.0 N NaOH / dioxane / 2 h / Ambient temperature

5: 52 percent / triethylamine, N,N'-dicyclohexylcarbodiimide / tetrahydrofuran / 6 h / Ambient temperature

With dmap; sodium hydroxide; sodium periodate; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00167a028