p-methoxybenzyl 3-exo-methylene-7-(phenylacetamido)-cepham-4-carboxylate

Base Information

Chemical Name:p-methoxybenzyl 3-exo-methylene-7-(phenylacetamido)-cepham-4-carboxylate
CAS No.:112020-52-7
Molecular Formula:C₂₄H₂₄N₂O₅S
Molecular Weight:452.531
Hs Code.:

Synonyms:p-methoxybenzyl 3-exo-methylene-7-(phenylacetamido)-cepham-4-carboxylate

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Chemical Property of p-methoxybenzyl 3-exo-methylene-7-(phenylacetamido)-cepham-4-carboxylate

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Technology Process of p-methoxybenzyl 3-exo-methylene-7-(phenylacetamido)-cepham-4-carboxylate

There total 10 articles about p-methoxybenzyl 3-exo-methylene-7-(phenylacetamido)-cepham-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 104146-10-3
(6R,7R)-3-Chloromethyl-8-oxo-7-phenylacetylamino-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid 4-methoxy-benzyl ester

: 112020-52-7
p-methoxybenzyl 3-exo-methylene-7-(phenylacetamido)-cepham-4-carboxylate

Guidance literature:: With ammonium perchlorate; lithium perchlorate; In tetrahydrofuran; water; for 1.4h; Ambient temperature; electroreduction (lead cathode, platinum anode);
DOI:10.1246/bcsj.59.3975

Reference yield: 76.0%

: p-methoxybenzyl 3-methoxymethyl-7-phenylacetamido-Δ3-cephem-4-carboxylate

: 112020-52-7
p-methoxybenzyl 3-exo-methylene-7-(phenylacetamido)-cepham-4-carboxylate

Guidance literature:: With samarium diiodide; tert-butyl alcohol; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 ℃; for 0.166667h;
DOI:10.1080/00397919308011140

Reference yield: 64.0%

: 101156-40-5
(6R,7R)-4-methoxybenzyl-3-(iodomethyl)-8-oxo-7-(2-phenylacetamido)-5-thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylate

: 29126-11-2
(6R,7R)-3-Methyl-8-oxo-7-phenylacetylamino-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid 4-methoxy-benzyl ester

: 112020-52-7
p-methoxybenzyl 3-exo-methylene-7-(phenylacetamido)-cepham-4-carboxylate

Guidance literature:: With ammonium perchlorate; lithium perchlorate; In tetrahydrofuran; water; Ambient temperature; electroreduction (lead cathode, platinum anode);
DOI:10.1246/bcsj.59.3975