C₃₈H₅₃NO₄

Base Information

Chemical Name:C₃₈H₅₃NO₄
CAS No.:1276112-37-8
Molecular Formula:C₃₈H₅₃NO₄
Molecular Weight:587.843
Hs Code.:

C<sub>38</sub>H<sub>53</sub>NO<sub>4</sub>

Synonyms:C₃₈H₅₃NO₄

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Chemical Property of C₃₈H₅₃NO₄

Chemical Property:

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Technology Process of C₃₈H₅₃NO₄

There total 20 articles about C₃₈H₅₃NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1276112-36-7
C₄₃H₆₁NO₆

: 1276112-37-8
C₃₈H₅₃NO₄

Guidance literature:: With hydrogenchloride; In methanol; water; at 20 ℃; for 12h;
DOI:10.1016/j.tetlet.2011.01.018

Reference yield:

: 1308271-84-2
C₂₇H₂₇NO₅

: 1276112-37-8
C₃₈H₅₃NO₄

Guidance literature:: Multi-step reaction with 15 steps

1: sodium tetrahydroborate / methanol / 24 h / 0 - 20 °C

2: silver(l) oxide / N,N-dimethyl-formamide / 24 h / 20 °C

3: ammonium cerium (IV) nitrate / water; acetonitrile / 2.5 h / 0 - 20 °C

4: dmap; triethylamine / dichloromethane / 2 h / 0 °C

5: tetrahydrofuran / 1.5 h / -78 °C

6: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 2 h / 0 °C

7: pyridine / 12 h / 0 - 20 °C

8: tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium formate; triethylamine / toluene / 0.5 h / Reflux

9: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone; tert-butyl alcohol / 24 h / 20 °C

10: sodium periodate / tetrahydrofuran; water / 3.5 h / 0 - 20 °C

11: t-butyldimethylsiyl triflate / toluene / 9 h / -78 °C

12: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone; tert-butyl alcohol / 24 h / 20 °C

13: sodium periodate / tetrahydrofuran; water / 4 h / 0 - 20 °C

14: tetrahydrofuran / 4.5 h / -78 - 0 °C / Inert atmosphere

15: hydrogenchloride / methanol; water / 12 h / 20 °C

With pyridine; hydrogenchloride; dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium cerium (IV) nitrate; cerium(III) chloride heptahydrate; t-butyldimethylsiyl triflate; ammonium formate; 4-methylmorpholine N-oxide; triethylamine; silver(l) oxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2011.01.018

Reference yield:

: 1308271-86-4
C₂₇H₂₉NO₅

: 1276112-37-8
C₃₈H₅₃NO₄

Guidance literature:: Multi-step reaction with 14 steps

1: silver(l) oxide / N,N-dimethyl-formamide / 24 h / 20 °C

2: ammonium cerium (IV) nitrate / water; acetonitrile / 2.5 h / 0 - 20 °C

3: dmap; triethylamine / dichloromethane / 2 h / 0 °C

4: tetrahydrofuran / 1.5 h / -78 °C

5: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 2 h / 0 °C

6: pyridine / 12 h / 0 - 20 °C

7: tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium formate; triethylamine / toluene / 0.5 h / Reflux

8: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone; tert-butyl alcohol / 24 h / 20 °C

9: sodium periodate / tetrahydrofuran; water / 3.5 h / 0 - 20 °C

10: t-butyldimethylsiyl triflate / toluene / 9 h / -78 °C

11: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone; tert-butyl alcohol / 24 h / 20 °C

12: sodium periodate / tetrahydrofuran; water / 4 h / 0 - 20 °C

13: tetrahydrofuran / 4.5 h / -78 - 0 °C / Inert atmosphere

14: hydrogenchloride / methanol; water / 12 h / 20 °C

With pyridine; hydrogenchloride; dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonium cerium (IV) nitrate; cerium(III) chloride heptahydrate; t-butyldimethylsiyl triflate; ammonium formate; 4-methylmorpholine N-oxide; triethylamine; silver(l) oxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2011.01.018