2,2-Dimethyl-propionic acid (S)-2-(3,4-dimethoxy-phenyl)-cyclohex-2-enyl ester

Base Information

Chemical Name:2,2-Dimethyl-propionic acid (S)-2-(3,4-dimethoxy-phenyl)-cyclohex-2-enyl ester
CAS No.:216006-02-9
Molecular Formula:C₁₉H₂₆O₄
Molecular Weight:318.413
Hs Code.:

Synonyms:2,2-Dimethyl-propionic acid (S)-2-(3,4-dimethoxy-phenyl)-cyclohex-2-enyl ester

Suppliers and Price of 2,2-Dimethyl-propionic acid (S)-2-(3,4-dimethoxy-phenyl)-cyclohex-2-enyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2,2-Dimethyl-propionic acid (S)-2-(3,4-dimethoxy-phenyl)-cyclohex-2-enyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2,2-Dimethyl-propionic acid (S)-2-(3,4-dimethoxy-phenyl)-cyclohex-2-enyl ester

There total 4 articles about 2,2-Dimethyl-propionic acid (S)-2-(3,4-dimethoxy-phenyl)-cyclohex-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 216005-83-3
2,2-Dimethyl-propionic acid (1S,2S)-2-(3,4-dimethoxy-phenyl)-2-hydroxy-cyclohexyl ester

: 216006-02-9
2,2-Dimethyl-propionic acid (S)-2-(3,4-dimethoxy-phenyl)-cyclohex-2-enyl ester

Guidance literature:: With Burgess Reagent; In toluene; at 50 ℃; for 1h;
DOI:10.1016/S0040-4039(98)01689-X

Reference yield:

: 27124-93-2
1-(3,4-dimethoxyphenyl)cyclohexene

: 216006-02-9
2,2-Dimethyl-propionic acid (S)-2-(3,4-dimethoxy-phenyl)-cyclohex-2-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / AD-mix-α, K2CO3, K3Fe(CN)6, MeSO2NH2 / 2-methyl-propan-2-ol; H2O / 48 h / Ambient temperature

2: 96 percent / Et₃N, DMAP / CH₂Cl₂ / 24 h / Ambient temperature

3: 98 percent / Et₃NSO₂NCO₂Me / toluene / 1 h / 50 °C

With dmap; AD-mix-α; Burgess Reagent; methanesulfonamide; potassium carbonate; triethylamine; potassium hexacyanoferrate(III); In dichloromethane; water; toluene; tert-butyl alcohol;
DOI:10.1016/S0040-4039(98)01689-X

Reference yield:

: Benzoic acid (1S,2S)-2-(3,4-dimethoxy-phenyl)-2-hydroxy-cyclohexyl ester

: 216006-02-9
2,2-Dimethyl-propionic acid (S)-2-(3,4-dimethoxy-phenyl)-cyclohex-2-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / NaOH / methanol / 4 h / Ambient temperature

2: 96 percent / Et₃N, DMAP / CH₂Cl₂ / 24 h / Ambient temperature

3: 98 percent / Et₃NSO₂NCO₂Me / toluene / 1 h / 50 °C

With dmap; sodium hydroxide; Burgess Reagent; triethylamine; In methanol; dichloromethane; toluene;
DOI:10.1016/S0040-4039(98)01689-X