2-N-methylanilino-2-(2-methyl-6-p-tolylsulphonylcyclohexyl)acetonitrile

Base Information

Chemical Name:2-N-methylanilino-2-(2-methyl-6-p-tolylsulphonylcyclohexyl)acetonitrile
CAS No.:117909-47-4
Molecular Formula:C₂₃H₂₈N₂O₂S
Molecular Weight:396.554
Hs Code.:

Synonyms:2-N-methylanilino-2-(2-methyl-6-p-tolylsulphonylcyclohexyl)acetonitrile

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Chemical Property of 2-N-methylanilino-2-(2-methyl-6-p-tolylsulphonylcyclohexyl)acetonitrile

Chemical Property:

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Technology Process of 2-N-methylanilino-2-(2-methyl-6-p-tolylsulphonylcyclohexyl)acetonitrile

There total 6 articles about 2-N-methylanilino-2-(2-methyl-6-p-tolylsulphonylcyclohexyl)acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 117909-46-3
(E)-4-Methyl-2-(methyl-phenyl-amino)-8-(toluene-4-sulfonyl)-oct-2-enenitrile

: 117909-47-4
2-N-methylanilino-2-(2-methyl-6-p-tolylsulphonylcyclohexyl)acetonitrile

Guidance literature:: With sodium methylate; In methanol; for 24h; Ambient temperature;

Reference yield:

: 100-61-8
N-methylaniline

: 117909-47-4
2-N-methylanilino-2-(2-methyl-6-p-tolylsulphonylcyclohexyl)acetonitrile

Guidance literature:: Multi-step reaction with 5 steps

1: 2.59 g / HCl / benzyltriethylammonium chloride / H₂O / 4 h / Ambient temperature

2: MeONa / methanol / 1 h / Ambient temperature

3: 1.) BuLi, di-isopropylamine, hexamethylphosphoric triamide / 1.) THF, hexane, -78 deg C, 45 min; 2.) THF, hexane

4: 91 percent / methanol / 6 h / Ambient temperature

5: 75 percent / MeONa / methanol / 24 h / Ambient temperature

With hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; sodium methylate; diisopropylamine; N-benzyl-N,N,N-triethylammonium chloride; In methanol; water;

Reference yield:

: 57361-03-2
(E/Z)-2-(N-Methylanilino)-2-pentennitril

: 117909-47-4
2-N-methylanilino-2-(2-methyl-6-p-tolylsulphonylcyclohexyl)acetonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) BuLi, di-isopropylamine, hexamethylphosphoric triamide / 1.) THF, hexane, -78 deg C, 45 min; 2.) THF, hexane

2: 91 percent / methanol / 6 h / Ambient temperature

3: 75 percent / MeONa / methanol / 24 h / Ambient temperature

With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; sodium methylate; diisopropylamine; In methanol;