benzyl 3,4,6-tri-O-benzyl-O-(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)-(1->2)-α-D-mannopyranoside

Base Information

Chemical Name:benzyl 3,4,6-tri-O-benzyl-O-(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)-(1->2)-α-D-mannopyranoside
CAS No.:479623-72-8
Molecular Formula:C₆₁H₆₄O₁₁
Molecular Weight:973.173
Hs Code.:

Synonyms:benzyl 3,4,6-tri-O-benzyl-O-(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)-(1->2)-α-D-mannopyranoside

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Chemical Property of benzyl 3,4,6-tri-O-benzyl-O-(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)-(1->2)-α-D-mannopyranoside

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Technology Process of benzyl 3,4,6-tri-O-benzyl-O-(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)-(1->2)-α-D-mannopyranoside

There total 7 articles about benzyl 3,4,6-tri-O-benzyl-O-(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)-(1->2)-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61134-30-3
benzyl 3,4,6-tri-O-benzyl-α-D-mannopyranoside

: 479623-72-8
benzyl 3,4,6-tri-O-benzyl-O-(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)-(1->2)-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / NIS; TBDMSOTf; 3 Angstroem molecular sieves / CH₂Cl₂

2: NaOMe

3: L-selectride

With N-iodo-succinimide; 3 A molecular sieve; t-butyldimethylsiyl triflate; sodium methylate; L-Selectride; In dichloromethane; 3: Swern oxidation;
DOI:10.1055/s-2003-40350

Reference yield:

: 479623-58-0
3,4,6-tri-O-benzyl-β-D-mannopyranose 1,2-(benzyl orthobenzoate)

: 479623-72-8
benzyl 3,4,6-tri-O-benzyl-O-(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)-(1->2)-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: TBDMSOTf

2: NaOMe

3: 92 percent / NIS; TBDMSOTf; 3 Angstroem molecular sieves / CH₂Cl₂

4: NaOMe

5: L-selectride

With N-iodo-succinimide; 3 A molecular sieve; t-butyldimethylsiyl triflate; sodium methylate; L-Selectride; In dichloromethane; 5: Swern oxidation;
DOI:10.1055/s-2003-40350

Reference yield:

: 479623-61-5
Benzoic acid (2S,3S,4S,5R,6R)-2,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-3-yl ester

: 479623-72-8
benzyl 3,4,6-tri-O-benzyl-O-(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)-(1->2)-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: NaOMe

2: 92 percent / NIS; TBDMSOTf; 3 Angstroem molecular sieves / CH₂Cl₂

3: NaOMe

4: L-selectride

With N-iodo-succinimide; 3 A molecular sieve; t-butyldimethylsiyl triflate; sodium methylate; L-Selectride; In dichloromethane; 4: Swern oxidation;
DOI:10.1055/s-2003-40350