10-(4-methoxyphenyl)-3-((E)-2-(10-(4-methoxyphenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazin-7-yl)vinyl)-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

Base Information

Chemical Name:10-(4-methoxyphenyl)-3-((E)-2-(10-(4-methoxyphenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazin-7-yl)vinyl)-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine
CAS No.:1357304-48-3
Molecular Formula:C₅₂H₅₂B₂N₂O₆S₂
Molecular Weight:886.749
Hs Code.:

10-(4-methoxyphenyl)-3-((E)-2-(10-(4-methoxyphenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazin-7-yl)vinyl)-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

Synonyms:10-(4-methoxyphenyl)-3-((E)-2-(10-(4-methoxyphenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazin-7-yl)vinyl)-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

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Chemical Property of 10-(4-methoxyphenyl)-3-((E)-2-(10-(4-methoxyphenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazin-7-yl)vinyl)-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

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Technology Process of 10-(4-methoxyphenyl)-3-((E)-2-(10-(4-methoxyphenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazin-7-yl)vinyl)-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

There total 6 articles about 10-(4-methoxyphenyl)-3-((E)-2-(10-(4-methoxyphenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazin-7-yl)vinyl)-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 61676-62-8
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1357304-47-2
3-bromo-7-((E)-2-(3-bromo-10-(4-methoxyphenyl)-10H-phenothiazin-7-yl)vinyl)-10-(4-methoxyphenyl)-10H-phenothiazine

: 1357304-48-3
10-(4-methoxyphenyl)-3-((E)-2-(10-(4-methoxyphenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazin-7-yl)vinyl)-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

Guidance literature:: 3-bromo-7-((E)-2-(3-bromo-10-(4-methoxyphenyl)-10H-phenothiazin-7-yl)vinyl)-10-(4-methoxyphenyl)-10H-phenothiazine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 2h;

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 13h;
DOI:10.1002/pola.25074

Reference yield:

: 1357304-46-1
7-bromo-10-(4-methoxyphenyl)-10H-phenothiazine-3-carbaldehyde

: 1357304-48-3
10-(4-methoxyphenyl)-3-((E)-2-(10-(4-methoxyphenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazin-7-yl)vinyl)-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: titanium tetrachloride; zinc / tetrahydrofuran / 12.5 h / -40 - 80 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C

2.2: 13 h / -78 - 20 °C

With n-butyllithium; titanium tetrachloride; zinc; In tetrahydrofuran; hexane;
DOI:10.1002/pola.25074

Reference yield:

: 58736-69-9
10-(4-methoxyphenyl)-10H-phenothiazine

: 1357304-48-3
10-(4-methoxyphenyl)-3-((E)-2-(10-(4-methoxyphenyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazin-7-yl)vinyl)-7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

Guidance literature:: Multi-step reaction with 4 steps

1.1: trichlorophosphate / 1,1,2-trichloroethane / 3.5 h / 0 - 95 °C

2.1: N-Bromosuccinimide / chloroform; acetic acid / 1 h / 65 °C

3.1: titanium tetrachloride; zinc / tetrahydrofuran / 12.5 h / -40 - 80 °C / Inert atmosphere

4.1: n-butyllithium / tetrahydrofuran; hexane / 2 h / -78 °C

4.2: 13 h / -78 - 20 °C

With N-Bromosuccinimide; n-butyllithium; titanium tetrachloride; zinc; trichlorophosphate; In tetrahydrofuran; hexane; chloroform; 1,1,2-trichloroethane; acetic acid;
DOI:10.1002/pola.25074