3-bromo-7-((E)-2-(3-bromo-10-(4-methoxyphenyl)-10H-phenothiazin-7-yl)vinyl)-10-(4-methoxyphenyl)-10H-phenothiazine

Base Information

Chemical Name:3-bromo-7-((E)-2-(3-bromo-10-(4-methoxyphenyl)-10H-phenothiazin-7-yl)vinyl)-10-(4-methoxyphenyl)-10H-phenothiazine
CAS No.:1357304-47-2
Molecular Formula:C₄₀H₂₈Br₂N₂O₂S₂
Molecular Weight:792.615
Hs Code.:

Synonyms:3-bromo-7-((E)-2-(3-bromo-10-(4-methoxyphenyl)-10H-phenothiazin-7-yl)vinyl)-10-(4-methoxyphenyl)-10H-phenothiazine

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Chemical Property of 3-bromo-7-((E)-2-(3-bromo-10-(4-methoxyphenyl)-10H-phenothiazin-7-yl)vinyl)-10-(4-methoxyphenyl)-10H-phenothiazine

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Technology Process of 3-bromo-7-((E)-2-(3-bromo-10-(4-methoxyphenyl)-10H-phenothiazin-7-yl)vinyl)-10-(4-methoxyphenyl)-10H-phenothiazine

There total 5 articles about 3-bromo-7-((E)-2-(3-bromo-10-(4-methoxyphenyl)-10H-phenothiazin-7-yl)vinyl)-10-(4-methoxyphenyl)-10H-phenothiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1357304-46-1
7-bromo-10-(4-methoxyphenyl)-10H-phenothiazine-3-carbaldehyde

: 1357304-47-2
3-bromo-7-((E)-2-(3-bromo-10-(4-methoxyphenyl)-10H-phenothiazin-7-yl)vinyl)-10-(4-methoxyphenyl)-10H-phenothiazine

Guidance literature:: With titanium tetrachloride; zinc; In tetrahydrofuran; at -40 - 80 ℃; for 12.5h; Inert atmosphere;
DOI:10.1002/pola.25074

Reference yield:

: 58736-69-9
10-(4-methoxyphenyl)-10H-phenothiazine

: 1357304-47-2
3-bromo-7-((E)-2-(3-bromo-10-(4-methoxyphenyl)-10H-phenothiazin-7-yl)vinyl)-10-(4-methoxyphenyl)-10H-phenothiazine

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate / 1,1,2-trichloroethane / 3.5 h / 0 - 95 °C

2: N-Bromosuccinimide / chloroform; acetic acid / 1 h / 65 °C

3: titanium tetrachloride; zinc / tetrahydrofuran / 12.5 h / -40 - 80 °C / Inert atmosphere

With N-Bromosuccinimide; titanium tetrachloride; zinc; trichlorophosphate; In tetrahydrofuran; chloroform; 1,1,2-trichloroethane; acetic acid;
DOI:10.1002/pola.25074

Reference yield:

: 104-92-7
1-bromo-4-methoxy-benzene

: 1357304-47-2
3-bromo-7-((E)-2-(3-bromo-10-(4-methoxyphenyl)-10H-phenothiazin-7-yl)vinyl)-10-(4-methoxyphenyl)-10H-phenothiazine

Guidance literature:: Multi-step reaction with 4 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate; tricyclohexylphosphine / toluene / 5 h / 120 °C / Inert atmosphere

2: trichlorophosphate / 1,1,2-trichloroethane / 3.5 h / 0 - 95 °C

3: N-Bromosuccinimide / chloroform; acetic acid / 1 h / 65 °C

4: titanium tetrachloride; zinc / tetrahydrofuran / 12.5 h / -40 - 80 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-Bromosuccinimide; titanium tetrachloride; sodium t-butanolate; zinc; trichlorophosphate; tricyclohexylphosphine; In tetrahydrofuran; chloroform; 1,1,2-trichloroethane; acetic acid; toluene;
DOI:10.1002/pola.25074