Technology Process of 2-(tert-butyldimethylsilyl)-4-hydroxy-4-methylcyclohexa-2,5-dienone
There total 3 articles about 2-(tert-butyldimethylsilyl)-4-hydroxy-4-methylcyclohexa-2,5-dienone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
4-tolyl iodide; water; 3-chloro-benzenecarboperoxoic acid;
In
acetonitrile;
at 20 - 25 ℃;
DOI:10.1039/c3cc00013c
- Guidance literature:
-
Multi-step reaction with 2 steps
1: n-butyllithium / tetrahydrofuran / 2 h / -78 - 20 °C / Inert atmosphere
2: 3-chloro-benzenecarboperoxoic acid; water; 4-tolyl iodide / acetonitrile / 20 - 25 °C
With
n-butyllithium; 4-tolyl iodide; water; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; acetonitrile;
DOI:10.1039/c3cc00013c
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1H-imidazole / dichloromethane / 0 - 20 °C
2: n-butyllithium / tetrahydrofuran / 2 h / -78 - 20 °C / Inert atmosphere
3: 3-chloro-benzenecarboperoxoic acid; water; 4-tolyl iodide / acetonitrile / 20 - 25 °C
With
1H-imidazole; n-butyllithium; 4-tolyl iodide; water; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1039/c3cc00013c
