(S)-3-<(4-methoxyphenyl)methoxy>-1,3-propanediol 1-(2,4,6-triisopropylbenzene sulfonate)

Base Information

Chemical Name:(S)-3-<(4-methoxyphenyl)methoxy>-1,3-propanediol 1-(2,4,6-triisopropylbenzene sulfonate)
CAS No.:109786-75-6
Molecular Formula:C₂₆H₃₈O₆S
Molecular Weight:478.65
Hs Code.:

Synonyms:(S)-3-<(4-methoxyphenyl)methoxy>-1,3-propanediol 1-(2,4,6-triisopropylbenzene sulfonate)

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Chemical Property of (S)-3-<(4-methoxyphenyl)methoxy>-1,3-propanediol 1-(2,4,6-triisopropylbenzene sulfonate)

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Technology Process of (S)-3-<(4-methoxyphenyl)methoxy>-1,3-propanediol 1-(2,4,6-triisopropylbenzene sulfonate)

There total 5 articles about (S)-3-<(4-methoxyphenyl)methoxy>-1,3-propanediol 1-(2,4,6-triisopropylbenzene sulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 6553-96-4
2,4,6-triisopropylphenylsulfonyl chloride

: 109786-74-5
(R)-3-(4-methoxybenzyloxy)propane-1,2-diol

: 109786-75-6
(S)-3-<(4-methoxyphenyl)methoxy>-1,3-propanediol 1-(2,4,6-triisopropylbenzene sulfonate)

Guidance literature:: With pyridine; for 36h;
DOI:10.1021/jm00393a022

Reference yield:

: 109786-73-4
(S)-4-[(4-methoxybenzyloxy)methyl]-2,2-dimethyl-1,3-dioxolane

: 109786-75-6
(S)-3-<(4-methoxyphenyl)methoxy>-1,3-propanediol 1-(2,4,6-triisopropylbenzene sulfonate)

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / HCl / methanol / 0.7 h

2: 80 percent / pyridine / 36 h

With pyridine; hydrogenchloride; In methanol;
DOI:10.1021/jm00393a022

Reference yield:

: 109786-76-7
(R)-4-(((4-methoxybenzyl)oxy)methyl)-2,2-dimethyl-1,3-dioxolane

: 109786-75-6
(R)-3-<(4-methoxyphenyl)methoxy>-1,3-propanediol 1-(2,4,6-triisopropylbenzene sulfonate)

Guidance literature:: Multi-step reaction with 2 steps

1: HCl / methanol / 0.7 h

2: pyridine / 36 h

With pyridine; hydrogenchloride; In methanol;
DOI:10.1021/jm00393a022