O-Benzoyl-N-(7-chlor-5-phenyl-3H-1,4-benzodiazepin-2-yl)-N-methylhydroxylamin

Base Information

Chemical Name:O-Benzoyl-N-(7-chlor-5-phenyl-3H-1,4-benzodiazepin-2-yl)-N-methylhydroxylamin
CAS No.:77176-05-7
Molecular Formula:C₂₃H₁₈ClN₃O₂
Molecular Weight:403.868
Hs Code.:

Synonyms:O-Benzoyl-N-(7-chlor-5-phenyl-3H-1,4-benzodiazepin-2-yl)-N-methylhydroxylamin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-Benzoyl-N-(7-chlor-5-phenyl-3H-1,4-benzodiazepin-2-yl)-N-methylhydroxylamin

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Technology Process of O-Benzoyl-N-(7-chlor-5-phenyl-3H-1,4-benzodiazepin-2-yl)-N-methylhydroxylamin

There total 2 articles about O-Benzoyl-N-(7-chlor-5-phenyl-3H-1,4-benzodiazepin-2-yl)-N-methylhydroxylamin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 98-88-4
benzoyl chloride

: 77175-99-6
N-(7-Chlor-5-phenyl-3H-1,4-benzodiazepin-2-yl)-N-methylhydroxylamin

: 77176-05-7
O-Benzoyl-N-(7-chlor-5-phenyl-3H-1,4-benzodiazepin-2-yl)-N-methylhydroxylamin

Guidance literature:: With triethylamine; In tetrahydrofuran; Ambient temperature;
DOI:10.1002/ardp.19803131106

Reference yield:

: 4547-02-8
7-chloro-1,3-dihydro-5-phenyl-2H-1,4-benzodiazepin-2-thione

: 77176-05-7
O-Benzoyl-N-(7-chlor-5-phenyl-3H-1,4-benzodiazepin-2-yl)-N-methylhydroxylamin

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / methanol / 1.5 h / Heating

2: 75 percent / Et₃N / tetrahydrofuran / Ambient temperature

With triethylamine; In tetrahydrofuran; methanol;
DOI:10.1002/ardp.19803131106