tetraphenylethylresorcin[4]arene

Base Information

• Chemical Name: tetraphenylethylresorcin[4]arene
• CAS No.: 118600-22-9
• Molecular Formula: C₆₀H₅₆O₈
• Molecular Weight: 905.1
• Mol file: 118600-22-9.mol

Synonyms:tetraphenylethylresorcin[4]arene

Chemical Property of tetraphenylethylresorcin[4]arene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tetraphenylethylresorcin[4]arene

There total 3 articles about tetraphenylethylresorcin[4]arene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

3-phenyl-propionaldehyde (104-53-0) + recorcinol (108-46-3) → tetraphenylethylresorcin[4]arene (118600-22-9)

Guidance literature:

With hydrogenchloride; In ethanol; for 72h; Heating;

DOI:10.1039/b715273f

Reference yield: 78.0%

3-phenyl-propionaldehyde (104-53-0) + recorcinol (108-46-3) → 2,8,14,20-tetrakis(2-phenylethyl)pentacyclo<19.3.1.13,7.19,13.115,19>octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaene-4,6,10,12,16,18,22,24-octol (118600-22-9)

Guidance literature:

With hydrogenchloride; In ethanol; water; at 0 - 20 ℃; for 72h; Reflux;

DOI:10.1002/ejoc.202001031

Reference yield:

3-phenyl-propenal (104-55-2) + recorcinol (108-46-3) → tetraphenylethylresorcin[4]arene (118600-22-9)

Guidance literature:

With hydrogenchloride; In ethanol;

DOI:10.1016/j.tet.2008.02.050

upstream raw materials:

3-phenyl-propenal

recorcinol

3-phenyl-propionaldehyde

Downstream raw materials:

1,21,23,25-tetrakis(2-phenylethyl)-2,20:3,19-dimetheno-1H,21H,23H,25H-bis<1,3>dioxocino<5,4-i:5',4'-i'>benzo<1,2-d:5,4-d'>-bis<1,3>benzodioxocin-7,11,15-triol

pentacyclo<19.3.1.1^3,7.1^9,13.1¹⁵¹⁹>octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaen-4,6,10,12,16,18,22,24-octol, 5,11,17,23-tetrabromo-2,8,14,20-tetrakis(2-phenylethyl)-

1,21,23,25-tetrakis(2-phenylethyl)-2,20:3,19-dimetheno-1H,21H,23H,25H-bis<1,3>dioxocino<5,4-i:5',4'-i'>benzo<1,2-d:5,4-d'>-bis<1,3>benzodioxocin-7,11-diol

1,21,23,25-tetrakis(2-phenylethyl)-2,20:3,19-dimetheno-1H,21H,23H,25H-bis<1,3>dioxocino<5,4-i:5',4'-i'>benzo<1,2-d:5,4-d'>-bis<1,3>benzodioxocin-7,15-diol

Refernces

• 1、 Gajjar, Jinal,Vekariya, Rajesh H.,Sharma, Vinay S.,Parekh, Hitesh. "“Synthesis, design and characterization of supramolecular self-assembly of calix[4]resorcinare substituted LCs”". . p. 48 - 58. Retrieved 2018.
• 2、 Ugono, Onome,Moran, Jason P.,Holman, K. Travis. "Closed-surface hexameric metal-organic nanocapsules derived from cavitand ligands". . p. 1404 - 1406. Retrieved 2008/12/21.