pent-4-en-1-yl 2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetate

Base Information

Chemical Name:pent-4-en-1-yl 2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetate
CAS No.:1019777-27-5
Molecular Formula:C₂₄H₂₄ClNO₄
Molecular Weight:425.912
Hs Code.:

Synonyms:pent-4-en-1-yl 2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pent-4-en-1-yl 2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetate

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Technology Process of pent-4-en-1-yl 2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetate

There total 1 articles about pent-4-en-1-yl 2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 821-09-0
n-Pent-4-enyl alcohol

: 53-86-1
[1-(4-chlorobenzoyl)-5-methoxy-2-methylindol-3-yl]acetic acid

: 1019777-27-5
pent-4-en-1-yl 2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1002/anie.201915837

Reference yield: 86.0%

: 1019777-27-5
pent-4-en-1-yl 2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetate

: 5720-07-0
4-methoxyphenylboronic acid

: 1019777-24-2
1-(4-(4'-methoxyphenyl)benzoyl)-5-methoxy-2-methylindole-3-acetic acid 4-pentenyl ester

Guidance literature:: With dichloro[1,1'-bis(di-t-butylphosphino)ferrocene]palladium(II); triethylamine; In water; at 50 ℃; for 24h; Inert atmosphere; Micellar solution;
DOI:10.1021/ol702714y

Reference yield: 80.0%

: 1019777-27-5
pent-4-en-1-yl 2-(1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl)acetate

: 102-01-2,98624-45-4
N-phenylacetoacetamide

: C₃₄H₃₅ClN₂O₆

Guidance literature:: With 1,2-bis(2,4,6-triisopropylphenyl)disulfane; [Ir(dF(CH₃)ppy)₂(dtbbpy)]BAr^F₄; C₁₁H₂₄BNO; at 25 - 30 ℃; for 48h; Inert atmosphere; Sealed tube; Irradiation;
DOI:10.1021/jacs.1c05852