(η6-bimesityl)(η6-benzene)chromium

Base Information

• Chemical Name: (η6-bimesityl)(η6-benzene)chromium
• CAS No.: 130085-93-7
• Molecular Formula: C₂₄H₂₈Cr
• Molecular Weight: 368.482
• Mol file: 130085-93-7.mol

Synonyms:(η6-bimesityl)(η6-benzene)chromium

Chemical Property of (η6-bimesityl)(η6-benzene)chromium

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of (η6-bimesityl)(η6-benzene)chromium

There total 1 articles about (η6-bimesityl)(η6-benzene)chromium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bimesityl (4482-03-5) + chromium (7440-47-3) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → bis(benzene)chromium(0) (1271-54-1) + (η6-bimesityl)(η6-benzene)chromium (130085-93-7) + bis(η6-bimesityl)chromium (130085-91-5)

Guidance literature:

In toluene; (N2); cocondensation of Cr, bimesityl and benzene during 1 h from a conic W-wire spiral and separation of heatable bimesityl and benzene vapour source in a static, evacuated reactor (cooled by N2(l)); warming to room temp.; addn. of solvent; filtration (silica gel); evapn. of solvent; sublimation of bimesityl, and compound 6 at 80°C; sublimation of compound 5 between 90-110°C; sublimation of complex 2 at 180°C;

DOI:10.1016/0022-328X(90)80174-X

upstream raw materials:

bimesityl

chromium

benzene

Refernces