C₁₉H₁₄BrCl₂NO₄

Base Information

Chemical Name:C₁₉H₁₄BrCl₂NO₄
CAS No.:1251583-58-0
Molecular Formula:C₁₉H₁₄BrCl₂NO₄
Molecular Weight:471.134
Hs Code.:

C<sub>19</sub>H<sub>14</sub>BrCl<sub>2</sub>NO<sub>4</sub>

Synonyms:C₁₉H₁₄BrCl₂NO₄

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Chemical Property of C₁₉H₁₄BrCl₂NO₄

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Technology Process of C₁₉H₁₄BrCl₂NO₄

There total 5 articles about C₁₉H₁₄BrCl₂NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1251583-57-9
C₁₈H₁₂BrCl₂NO₄

: 74-88-4
methyl iodide

: 1251583-58-0
C₁₉H₁₄BrCl₂NO₄

Guidance literature:: C₁₈H₁₂BrCl₂NO₄; With caesium carbonate; In dimethyl sulfoxide; at 20 ℃; for 0.0833333h;

methyl iodide; In dimethyl sulfoxide; at 45 ℃; for 0.75h;

Reference yield:

: 1251583-16-0
C₁₈H₁₂Cl₂N₂O₆

: 1251583-58-0
C₁₉H₁₄BrCl₂NO₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; tin / tetrahydrofuran / 4 h / Inert atmosphere; Reflux

2.1: tert.-butylnitrite; copper(ll) bromide / acetonitrile / 3 h / 20 °C

3.1: caesium carbonate / dimethyl sulfoxide / 0.08 h / 20 °C

3.2: 0.75 h / 45 °C

With hydrogenchloride; tin; tert.-butylnitrite; caesium carbonate; copper(ll) bromide; In tetrahydrofuran; dimethyl sulfoxide; acetonitrile;

Reference yield:

: 1251583-55-7
C₁₈H₁₄Cl₂N₂O₄

: 1251583-58-0
C₁₉H₁₄BrCl₂NO₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert.-butylnitrite; copper(ll) bromide / acetonitrile / 3 h / 20 °C

2.1: caesium carbonate / dimethyl sulfoxide / 0.08 h / 20 °C

2.2: 0.75 h / 45 °C

With tert.-butylnitrite; caesium carbonate; copper(ll) bromide; In dimethyl sulfoxide; acetonitrile;