4-hexylthio-5-(4-phenyloxyacetic acid)phthalonitrile

Base Information

Chemical Name:4-hexylthio-5-(4-phenyloxyacetic acid)phthalonitrile
CAS No.:1204533-34-5
Molecular Formula:C₂₂H₂₂N₂O₃S
Molecular Weight:394.494
Hs Code.:

Synonyms:4-hexylthio-5-(4-phenyloxyacetic acid)phthalonitrile

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Chemical Property of 4-hexylthio-5-(4-phenyloxyacetic acid)phthalonitrile

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Technology Process of 4-hexylthio-5-(4-phenyloxyacetic acid)phthalonitrile

There total 1 articles about 4-hexylthio-5-(4-phenyloxyacetic acid)phthalonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.7%

: 111-31-9
Hexanethiol

: 1204533-18-5
4-chloro-5-(4-phenyloxyacetic acid)phthalonitrile

: 1204533-34-5
4-hexylthio-5-(4-phenyloxyacetic acid)phthalonitrile

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.jorganchem.2009.09.025

Reference yield: 27.0%

: 1204533-34-5
4-hexylthio-5-(4-phenyloxyacetic acid)phthalonitrile

: 1204533-35-6
2,9,16,23-tetra(hexylthio)-3,10,17,24-tetra(4-phenyloxyacetic acid)-phthalocyaninatozinc(II)

Guidance literature:: With zinc(II) acetate dihydrate; In 2-(N,N-dimethylamino)ethanol; at 160 ℃; for 24h; Inert atmosphere; sealed glass tube;
DOI:10.1016/j.jorganchem.2009.09.025

Reference yield: 27.0%

: 1204533-34-5
4-hexylthio-5-(4-phenyloxyacetic acid)phthalonitrile

: 5970-45-6
zinc(II) acetate dihydrate

: 1204533-35-6
2,9,16,23-tetra(hexylthio)-3,10,17,24-tetra(4-phenyloxyacetic acid)-phthalocyaninatozinc(II)

Guidance literature:: In further solvent(s); 2-(dimethylamino)ethanol as solvent, mixt. of phthalonitrile, Zn(OAc)2 and dimethylethanol heated and stirred at 160°C for 24 h under N2,cooling to room temp. and treated with dild. HCl; ppt. centrifuged, washed (H2O, until neutral washings), dissolved in THF, pptd. with chloroform, washed (CHCl3); elem. anal.;
DOI:10.1016/j.jorganchem.2009.09.025