2,9,16,23-tetra(hexylthio)-3,10,17,24-tetra(4-phenyloxyacetic acid)-phthalocyaninatozinc(II)

Base Information

Chemical Name:2,9,16,23-tetra(hexylthio)-3,10,17,24-tetra(4-phenyloxyacetic acid)-phthalocyaninatozinc(II)
CAS No.:1204533-35-6
Molecular Formula:C₈₈H₈₈N₈O₁₂S₄Zn
Molecular Weight:1643.37
Hs Code.:

Synonyms:2,9,16,23-tetra(hexylthio)-3,10,17,24-tetra(4-phenyloxyacetic acid)-phthalocyaninatozinc(II)

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Chemical Property of 2,9,16,23-tetra(hexylthio)-3,10,17,24-tetra(4-phenyloxyacetic acid)-phthalocyaninatozinc(II)

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Technology Process of 2,9,16,23-tetra(hexylthio)-3,10,17,24-tetra(4-phenyloxyacetic acid)-phthalocyaninatozinc(II)

There total 2 articles about 2,9,16,23-tetra(hexylthio)-3,10,17,24-tetra(4-phenyloxyacetic acid)-phthalocyaninatozinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 1204533-34-5
4-hexylthio-5-(4-phenyloxyacetic acid)phthalonitrile

: 1204533-35-6
2,9,16,23-tetra(hexylthio)-3,10,17,24-tetra(4-phenyloxyacetic acid)-phthalocyaninatozinc(II)

Guidance literature:: With zinc(II) acetate dihydrate; In 2-(N,N-dimethylamino)ethanol; at 160 ℃; for 24h; Inert atmosphere; sealed glass tube;
DOI:10.1016/j.jorganchem.2009.09.025

Reference yield: 27.0%

: 1204533-34-5
4-hexylthio-5-(4-phenyloxyacetic acid)phthalonitrile

: 5970-45-6
zinc(II) acetate dihydrate

: 1204533-35-6
2,9,16,23-tetra(hexylthio)-3,10,17,24-tetra(4-phenyloxyacetic acid)-phthalocyaninatozinc(II)

Guidance literature:: In further solvent(s); 2-(dimethylamino)ethanol as solvent, mixt. of phthalonitrile, Zn(OAc)2 and dimethylethanol heated and stirred at 160°C for 24 h under N2,cooling to room temp. and treated with dild. HCl; ppt. centrifuged, washed (H2O, until neutral washings), dissolved in THF, pptd. with chloroform, washed (CHCl3); elem. anal.;
DOI:10.1016/j.jorganchem.2009.09.025