C₃₀H₂₉ClN₆O₂

Base Information

Chemical Name:C₃₀H₂₉ClN₆O₂
CAS No.:1307853-62-8
Molecular Formula:C₃₀H₂₉ClN₆O₂
Molecular Weight:541.052
Hs Code.:

C<sub>30</sub>H<sub>29</sub>ClN<sub>6</sub>O<sub>2</sub>

Synonyms:C₃₀H₂₉ClN₆O₂

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Chemical Property of C₃₀H₂₉ClN₆O₂

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Technology Process of C₃₀H₂₉ClN₆O₂

There total 10 articles about C₃₀H₂₉ClN₆O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1301606-95-0
{2'-[1-(o-methoxybenzyl)-1H-tetrazol-5-yl]biphenyl-4-yl}-methanol

: 83857-96-9
2-n-butyl-4-chloro-1H-imidazol-5-carboxaldehyde

: 1307853-62-8
C₃₀H₂₉ClN₆O₂

Guidance literature:: {2'-[1-(o-methoxybenzyl)-1H-tetrazol-5-yl]biphenyl-4-yl}-methanol; With trimethylsilyl bromide; In acetonitrile; at 50 - 60 ℃; for 7h;

2-n-butyl-4-chloro-1H-imidazol-5-carboxaldehyde; With potassium carbonate; In acetonitrile; at 50 ℃; for 3h;

Reference yield:

: 143572-98-9
N-(2-methoxybenzyl)-benzoylamide

: 1307853-62-8
C₃₀H₂₉ClN₆O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: phosphorus pentachloride / dichloromethane / 2.18 h / -15 - 21 °C

1.2: -13 - 20 °C

2.1: potassium carbonate; triphenylphosphine / poly[(η²,η²-cycloocta-1,5-diene)ruthenium-di-β-chloro] / 1-methyl-pyrrolidin-2-one / 9 h / 140 °C / Inert atmosphere

3.1: ethanol; calcium chloride; sodium tetrahydroborate / 5.5 h / 20 - 60 °C

4.1: trimethylsilyl bromide / acetonitrile / 7 h / 50 - 60 °C

4.2: 3 h / 50 °C

With sodium tetrahydroborate; ethanol; trimethylsilyl bromide; phosphorus pentachloride; potassium carbonate; triphenylphosphine; calcium chloride; poly[(η²,η²-cycloocta-1,5-diene)ruthenium-di-β-chloro]; In 1-methyl-pyrrolidin-2-one; dichloromethane; acetonitrile;

Reference yield:

: 6850-57-3
2-methoxybenzylamine

: 1307853-62-8
C₃₀H₂₉ClN₆O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium carbonate / toluene; water / 3 - 20 °C

2.1: phosphorus pentachloride / dichloromethane / 2.18 h / -15 - 21 °C

2.2: -13 - 20 °C

3.1: potassium carbonate; triphenylphosphine / poly[(η²,η²-cycloocta-1,5-diene)ruthenium-di-β-chloro] / 1-methyl-pyrrolidin-2-one / 9 h / 140 °C / Inert atmosphere

4.1: ethanol; calcium chloride; sodium tetrahydroborate / 5.5 h / 20 - 60 °C

5.1: trimethylsilyl bromide / acetonitrile / 7 h / 50 - 60 °C

5.2: 3 h / 50 °C

With sodium tetrahydroborate; ethanol; trimethylsilyl bromide; phosphorus pentachloride; sodium carbonate; potassium carbonate; triphenylphosphine; calcium chloride; poly[(η²,η²-cycloocta-1,5-diene)ruthenium-di-β-chloro]; In 1-methyl-pyrrolidin-2-one; dichloromethane; water; toluene; acetonitrile;