ethyl 3-amino-3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)propionate

Base Information

Chemical Name:ethyl 3-amino-3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)propionate
CAS No.:1372195-43-1
Molecular Formula:C₂₆H₂₉NO₃
Molecular Weight:403.521
Hs Code.:

Synonyms:ethyl 3-amino-3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)propionate

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Chemical Property of ethyl 3-amino-3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)propionate

Chemical Property:

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Technology Process of ethyl 3-amino-3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)propionate

There total 3 articles about ethyl 3-amino-3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1071-46-1
hydrogen ethyl malonate

: 1372195-41-9
4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)benzaldehyde

: 1372195-43-1
ethyl 3-amino-3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)propionate

Guidance literature:: With ammonium acetate; In ethanol; for 20h; Reflux;

Reference yield:

: 691905-27-8
(2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methanol

: 1372195-43-1
ethyl 3-amino-3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)propionate

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / toluene; tetrahydrofuran / 15 h / 20 °C / Cooling with ice

2: ammonium acetate / ethanol / 20 h / Reflux

With di-isopropyl azodicarboxylate; ammonium acetate; triphenylphosphine; In tetrahydrofuran; ethanol; toluene;

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1372195-43-1
ethyl 3-amino-3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)propionate

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / toluene; tetrahydrofuran / 15 h / 20 °C / Cooling with ice

2: ammonium acetate / ethanol / 20 h / Reflux

With di-isopropyl azodicarboxylate; ammonium acetate; triphenylphosphine; In tetrahydrofuran; ethanol; toluene;